LAMPIRAN -1 PROSEDUR ANALISA

LAMPIRAN -1 PROSEDUR ANALISA

Universitas Sumatera Utara

LAMPIRAN -1A PROSEDUR ANALISA WARNA LOVIBOND

1. Tujuan Metode ini menentukan warna dengan membandingkan cahaya yang dipancarkan melalui kedalaman tertentu dari lemak, minyak atau asam lemak terhadap warna cahaya asal dari sumber yang sama, dipancarkan melalui standart.

2. Batasan Dapat digunakan untuk minyak-minyak hewan, tumbuh-tumbuhan dan asam lemak

3. Peralatan 3.1. Lovibond Tintometer Model E AF 900 3.2. Lighting cabinet, two 60 watt pearls lamps 3.3. Color racks, consisting of red, yellow, blue, and neutral Racks with color reading as follow Red : 0.1-0.9; 1.0-9.0; 10.0-70.0 Yellow

: 0.1-0.9; 1.0-9.0; 10.0-70.0

Blue

: 0.1-0.9; 1.0-9.0; 10.0-04.0

Neutral

: 0.1-0.9; 1.0-3.0

3.4. Glass cell, made of optical glass, 1" and 5.25"

4. Bahan-bahan: None Applicable


5. Langkah kerja 5.1. Cairkan contoh 100 C diatas titik leleh jika masih padat dan saring jika perlu untuk menghilangkan pengotor padat 5.2. Tuangkan contoh yang tersedia secukupnya ke dalam sel bersih dan kering 5.3. Tempatkan sel yang mengandung contoh kedalam pemegang sel secara benar. 5.4. Setelah penutupan ruang sel, segera tentukan warna contoh. Mula-mula digunakan rak warna kuning 10 terhadap merah 1. 5.5. Atur sampai perbandingan warna yang akurat dicapai, tanpa perlu mempertahankan ratio 10 kuning terhadap 1 merah dan gunakan angka biru atau netral yang rendah untuk memperoleh perbandingan, tapi tidak lebih dari 9.0 biru atau 3.0 netral 5.6. Mencatat ukuran cell dan pembacaan warna merah, kuning, biru atau netral pada pembentukan perbandingan warna. 5.7. Hasil dinyatakan dalam bentuk seperti dibawah ini : 5.7.1. Pembacaan angka merah, kuning, dan biru atau netral diperlukan untuk memperoleh perbandingan 5.7.2. Panjang sell yang digunakan 5.8. Pengukuran warna diambil pada satu panjang sel tidak boleh dipakai untuk menghitung nilai warna untuk panjang sell yang lain. 5.9. Sebaiknya ketajaman (kejelasan) warna tidak pernah lebih besar dari 20 total lovibond color 6. Rujukan AOCS Ce 13e-92


LAMPIRAN -1B PROSEDUR PEMBUATAN METYL ESTER ASAM LEMAK.

1. Tujuan Metil ester dari asam lemak dan minyak dipisahkan dan ditentukan secara kuantitatif dengan GLC menggunakan packed column tertentu atau asam lemak langsung dipisah dan ditentukan secara kuantitatif dengan GLC menggunakan capillary column tertentu.

2. Batasan Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom karbon 6 sampai 20 setelah dirubah menjadi ester untuk packed atau langsung asam lemak untuk capillary column.

3. Peralatan 3.1. Analytical balance 3.2. Block heater 3.3. Thermometer 3.4. Screw vial, 5 ml

4. Bahan-bahan 4.1. BF 3 = methanol solution, reagent grade 4.2. Sodium chlorida saturated solution 4.3. Solvent, n-hexane, reagent grade 4.4. Methanol, reagent grade Universitas Sumatera Utara

4.5. NaOH 0.5 N in methanol Larutkan 20 +0.05 g, reagent grade NaOH dalam 1 L metanol

5. Langkah kerja 5.1. Determination carbon chain for fats and oils 5.1.1

Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup

5.1.2

Tambahkan 2 ml 0.05N NaOH – metanol, dan panaskan didalam blok pemanas pada suhu yang diatur 68+ 10C selama 10 menit.

5.1.3

Tambahkan 2 ml larutan reagen BF 3 metanol, dan panaskan didalam blok pemanas pada suhu yang diatur 68+ 10C selama 15 menit

5.1.4

Keluarkan dari blok pemanas dan didinginkan pada suhu ruangan

5.1.5

Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan biarkan selama 1 menit, sekarang larutan heksan siap di injeksikan.

5.2. Determination carbon chain ini pack column 5.2.1. Timbang sampel sekitar 0.02 ml gram kedalam vial 5 ml yang tertutup. 5.2.2. Tambahkan 2 ml larutkan reagen BF 3 metanol, dan panaskan didalam blok pemanas pada suhu yang diatur 68 + 10C selama 15 menit 5.2.3. Keluarkan dari blok pemanas dan dinginkan pada suhu ruangan. 5.2.4. Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan biarkan selama 2 menit, sekarang larutan heksan siap untuk di injeksikan. 5.3. Determination carbon chain ini capillary column 5.3.1. Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup 5.3.2. Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut panaskan beberapa menit untuk melarutkannya. 5.3.3. Sekarang larutan heksan siap untuk di injeksikan.

6. Rujukan AOCS CE2-66


LAMPIRAN -1C. PROSEDUR ANALISA KOMPOSISI ASAM LEMAK

1. Tujuan Metil ester dari asam lemak dipisahkan dan ditentukan secara kuantitatif dengan GLC menggunakan packed colomn tertentu asam lemak langsung dipisah dan ditentukan secara kuantitatif dengan GLC menggunakan capillary coloumn tertentu.

2. Batasan Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom karbon 6 sampai 20 setelah dirubah menjadi metil ester untuk packed column atau langsung asam lemak untuk capillary column.

3. Peralatan 3.1. Syringe, 10 1 3.2. Shimadzu Gas chromatograph, GC-14B 3.2.1. Injector – Insert glass type, splitless mode 3.2.2. Detector – Flame Ionization detector, range 102 3.2.3. Columns For methyl esters of fatty acid- GP 10% SP 216 PS on 100/120 Supelcoport. Supelco Cat. No. 1-1879, square Loop Universitas Sumatera Utara

For fatty acids : -

HP-FFAP, Cross linked polyethylene glycol-TPA phase 15 m x 0.53 mm x 1.0 m, Hawlett Packard Part No. 19095F 123

-

Coloum Glass, 20% DEGS Chromosorb WHP on 60/80 Temp. Max 2000C, P/N 221-14368-31/7G (3.2-3.1), Lenght 3 M

-

Coloum Stainless, GP 10% SP-216-PS on 100/120 Supelcoport Temp. Max 2000C, Lenght 2 M

Flow rate of Gas : Gases Packed Kpa Nitrogen 90 Hydrogen 60 Air 50 Temperature Programs Injector, 0C Detector0C Samples Column, 0C Initial temp, 0C Initial time, min. Program rate, 0C/min Final temp. 0C Final time, min

Capilllary KPa 40 55 30

Packed 220 230 CPO C 12 PKO RBD PS C 18 120 140 100 0 0 0 10 10 10 190 190 190 15 15 15

Capillary 230 250 C 8 -C 10 C 8, C 18

C 16 -C 18 170 0 10 190 8

100 0 10 230 5

3.3. Recording system, Chromatopac C-R6A Attenuation, mV/full scale

5

Width

0

Slope, V/min

70 max

Drift

0

Minimum Area, Count

1000 max

TDBL

0

Chart speed, mm/min

5

3.4. Screw –cap vial, 5 ml 3.5. Analytical balance, 0.0001 g accuracy

4. Bahan-bahan 4.1. Solvent,n-hexane, reagent grade Universitas Sumatera Utara

4.2. Carries gas, nitrogen with ultra high purity (UHP) 4.3. Hydrogen, Ultra high purity 4.4. Air, industrial grade, free from oil and moisture

5. Langkah Kerja 5.1. Preparation sample 5.1.1. Methyl ester 5.1.1.1.Penyediaan metil ester merujuk pada lampiran 6 5.1.2. Fatty Acid 5.1.2.1.Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang bertutup. 5.1.2.2.Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut panaskan beberapa menit untuk melarutkannya. 5.2. Prosedur 5.2.1. Pilih keadaan yang optimal dari sistem GC dan file Chromatopact untuk sampel yang tepat 5.2.2. Dengan menggunakan, injeksikan 1 kedalam kolom, dan start GC. 5.2.3. Identifikasikan puncak-puncak dari kromatogram, menggunakan kromatogram standar sebagai petunjuk. 5.3. Perhitungan ACi x FCi x 100 Calculation : % Ci = Sum (FCi x ACi

Dimana

% Ci

= Kandungan rantai karbon i dalam % berat

ACi

= Area rantai karbon i

FCi

= Faktor respons rantai karbon i

Sum (ACixFCi) = jumlah dari FCi x Aci

6. Rujukan 6.1. User Manual, Shimadzu Chromatopac C – R6A & C-R8A 6.2. User Manual, Shimadzu Chromatograph GC – 14B Universitas Sumatera Utara

7. Informasi-informasi lain yang dibutuhkan 1.1. Packed column hanya sesuai untuk metil ester 1.2. HP-FFAP untuk C8C10 Fatty Acid

LAMPIRAN -1D PEMBUATAN LARUTAN STANDAR NATRIUM TIOSULFAT (NA 2 S 2 O 3 ) 1. Tujuan Cara ini menunjukkan pembuatan dan membakukan larutan natrium tiosulfat secara kuantitatif.

2. Batasan Hanya dapat digunalan untuk larutan Natrium Thiosulfat

3. Peralatan 3.1. Analytical balance, 0.0001 g accuracy 3.2. Burrete, accurately calibrate 50 ml 3.3. Cylinder glass, 25 ml, 100 ml 3.4. Reagent bottle, 5000 ml 3.5. Volumetric pipette, 5 ml 3.6. Erlenmeyer flask, 300 ml 3.7. Volumetric dispenser 20 ml

4. Bahan-bahan 4.1. CO 2 free distilled water


Didihkan air suling selama 20 menit dan dinginkan dengan penutup untuk mencegah penyerapan CO 2 . 4.2. Potasium Iodium solution, 15% Larutkan 150 gram Kalium Iodium ke dalam 1000 ml air suling 4.3. Starch Indicator, 1% Larutkan 1 gram serbuk starch ke dalam 100 ml air suling yang panas dan dinginkan. 4.4. Standart primer kalium dikromat 0.1 N 4.5. Larutkan 2.4518 gram yang telah dikeringkan dan dinginkan dalam labu ukur 500 ml dengan air destilat dan terakan sampai tanda batas dan simpan dalam botol gelap. 5. Langkah Kerja 5.1. Preparation of Sodium solution, 0.1N & 0.01N Larutkan dalam 124,5 + 0.1 gr Natrium thisulfat ke dalam air suling dan larutkan hingga 5 L. 5.2. Sodium Thiosulfate Standardization 0.1N Pipet 25 ml larutan kalium dichromat ke dalam erlenmeyer 300 ml, tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodida dan aduk. Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air suling. Titrasi dengan larutan natrium thiosulfat, aduk sampai warna kuning pucat. Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara perlahan hingga warna biru benar benar tak kelihatan. 5.3. Sodium Thiosulfat Standardization 5.4. Encerkan 100 ml larutan N 2 S 2 O 3 0,1N ke dalam 1000 ml labu ukur dengan air destillat dan terakan sampai tanda batas. Untuk standarisasi, pipet 2 ml larutan kalium dichromat ke dalam erlenmeyer 300 ml . Tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodium dan aduk. Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air suling. Titrasi dengan larutan natrium thiosulfat, aduk sampai warna kuning pucat. Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara perlahan hingga warna biru benar-benar tak kelihatan. 5.5. Perhitungan Universitas Sumatera Utara

20.394 x wt of K 2 Cr 2 O 7 x fp ml of Na 2 S 2 O 3 Normality of Na 2 SO 2 O 3 =

6. Rujukan AOCS Official Method Tg 1-64.

LAMPIRAN -1E PEMBUATAN LARUTAN STANDAR WIJS

1. Tujuan Prosedur ini menggambarkan pembuatan larutan wijs dari iodine monochlorida

2. Batasan Cara ini hanya digunakan untuk membuat larutan wijs dari iodine monochlorida komersil.

3. Peralatan 3.1. Cylinder glass, 100, 1000 ml 3.2. Erlenmeyer flask, 500 ml 3.3. Filter paper 3.4. Magnetic stirrer 3.5. Reagent bottle, 5000 ml, amber 3.6. Volumentric pippete, 10 ml

4. Bahan-bahan 4.1. Acetic acid glacial Universitas Sumatera Utara

4.2. Distilled water 4.3. Iodine monochloride 4.4. Potasium Iodida Solution, 15% 4.5. Cyclo hexane 4.6. Starch indikator 4.7. Sodium thiodulfate solution, 0.1N 4.8. Sulfuric acid, 2%

5. Langkah kerja 5.1. Stock solution : Tambahkan 317 +0.1 g iodine monochloride ke 1 L asam asetat glasial, aduk hingga larut selanjutnya saring dengan kertas saring whatman 41H atau sejenisnya ke botol yang bersih dan kering. Saring dengan segera untuk mencegah terjadinya kontaminasi terhadap air dan simpan di tempat yang sejuk. Buang larutan bila terbentuk endapan. 5.2. Wijs Solution : Dengan menggunakan glas ukur tuangkan 117.0 + 0.1 ml larutan stock ke botol 5 L yang telah terisi asam asetat, kemudian aduk hingga merata. 5.3. Wijs standardization Menentukan perbandingan I/Cl yang mana harus dalam batas 1.10 + 0.1 seperti prosedur berikut : 5.3.1. Iodine content : Tuangkan 150 ml larutan chroline jenuh ke dalam erlenmeyer 500 ml, dan tambahkan beberapa butir butiran kaca. 5.3.2. Pipet 5 ml larutan wijs ke dalam larutan erlenmeyer yang telah berisi chlorine jenuh, aduk dan panaskan hingga mendidih. 5.3.3. Didihkan dengan cepat selama 10 menit, dinginkan dan tambahkan 30 ml asam sulfat 2% dan 15 ml larutan iodida. 5.3.4. Aduk dengan baik dan segera titrasi dengan larutan natrium thiosulfat 0.1N dengan starch sebagai indikator. 5.4. Total Halogen Content 5.4.1. Tuangkan 150 ml air destillat yang baru mendidih ke erlenmeyer 500 ml yang bersih dan kering. Universitas Sumatera Utara

5.4.2. Tambahkan 15 ml larutan kalium iodida 15% 5.4.3. Pipet 20 ml larutan Wijs ke dalam erlenmeyer tersebut, aduk hingga homogen 5.4.4. Titrasi dengan natrium tiosulfat 0.2N dengan starch sebagai indikator. 5.5. Perhitungan : Halogen ratio : Dimana :

2A 3B – 2A

A = Volumen natrium thiosulfat untuk menitrasi kandungan iodine B = Volume natrium thiosulfat untuk menitrasi kandungan halogen total.

6. Rujukan AOCS Official Method Tg 1-64


LAMPIRAN -1F PROSEDUR ANALISA BILANGAN IODIUM

1. Tujuan Bilangan iodine adalah suatu ukuran ketidakjenuhan dari minyak industri dan turunnya dan dinyatakan dalamistilah gram iodin terserap setiap 100 gram contoh (% iodine terserap).

2. Batasan Dapat digunakan untuk minyak-minyak industri dan turunnya, seperti minyak kering alami atau buatan dan asam lemaknya.

3. Peralatan 3.1. Analytical balance, accurate up to 0.0001 gr 3.2. Burrete or Automatic piston burrete with stirrer, 50 ml 3.3. Erlenmeyer flask with stopper, 250 to 300 ml 3.4. Volumetric dispenser, 30 ml, 1 ml adjustabilty 3.5. Volumetric pippete, 15,25 ml 3.6. Graduate cylinder, 100 ml

4. Bahan-bahan 4.1. Sodium Thiosulfate Solution. 0,1N Merujuk ke pada lampiran 8 4.2. Wijs Solution Merujuk pada lampiran 9 4.3. Pottasium Iodida Solution, 15% Larutkan 150 g kalium Iodida dalam 1000 ml air demin 4.4. Starch indicator solution Buat pasta 1 gram starch dengan sedikit air dingin. Tambahkan sambil diaduk dengan 100 ml air mendidih. 4.5. Sikloheksana sebagai pengganti karbon tetraklorida seperti rekomendasi


5. Langkah Kerja 5.1. Cairkan sampel jika masih padat dan timbang seperti berikut ini : (catatan 7). Sample Caprylic, Capric Aicd, Lauric Acid, Myristic Acid, TPSA, Hydrogenated, TPSA, DPSA, RGSA, Stearic 65%

Weight,g

5 + 0.5

Sample

Weight,g

CPKO, SPKOFA

0.70-1.00

RBDPS, SRBDPSFA

0.40-0.60

CPS, SCPSA and Oleic Acid

0.30-0.50

CPO, SPOFA

0.10-0.20

5.2. Tambahkan 10 ml Sikloheksana, pipet 15 ml larutan Wijs dalam labu yang mengandung contoh dan aduk dengan baik 5.3. Buat dan lakukan penentuan blanko sekaligus sama dengan contoh. 5.4. Simpan labu-labu di dalam tempat gelap selama 30 menit pada suhu 25 + 50C 5.5. Pindahkan labu ke penyimpanan, tambahkan 10 ml larutan Kl, 100 ml air suling. 5.6. Titrasi dengan larutan 0.1N Na 2 S 2 O 3 , penambahannya secara bertahap dan dengan pengadukan yang kuat dan tetap sampai warna kuning hampir lenyap. Tambahkan 1-2 larutan indikator kanji dan lanjutkan titrasi sampai warna biru lenyap seketika. 5.7. Perhitungan : Iodine value, gI 2 /100g Where :

( Vb – Vs) x N x 12.69 = W

Vb

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi blanko

Vs

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi contoh

N

= Normalitas Na 2 S 2 O 3

W

= Gram contoh

6. Rujukan AOCS Official Method Tg 1-64

7. Informasi-informasi lain yang dibutuhkan 7.1. Larutan Wijs harus lebih 100-150% terhadap jumlah terserap Universitas Sumatera Utara

7.2. Untuk Oleic acid, menggunakan 25 ml larutan Wijs, 20 ml Cyclohexane dan 20 ml larutan Kl 15% LAMPIRAN -1G PROSEDUR ANALISA HEAT STABILITY

1. Tujuan Metode ini mengukur stabilitas warna dari asam lemak (fatty acid) setelah pemanasan dalam kondisi analisa khusus.

2. Batasan Berlaku untuk semua fatty acid normal

3. Peralatan Oil batch Mixer Thermometer Tubes Thermal Resistance Filter paper Colorimeter

4. Bahan-bahan 4.1. Sulfuric Acid (corrosive material)

5. Langkah Kerja 5.1. Pembuatan larutan khusus Asam sulfat 1 : 1 Masukkan 1 bagian asam sulfat ke dalam 1 bagian air dengan hati – hati, jangan sampai terbalik. 5.2. Perlakuan Sampel Jika sampel yang diuji tidak cair pada suhu ruangan, cairkan dengan pemanasan di water batch sampai suhu tidak lebih dari 10 oC di atas titer sampel. Universitas Sumatera Utara

5.3. Perlakuan Peralatan 5.3.1. Pastikan sebelum oil batch digunakan, sudah diverifikasi dahulu suhunya dengan menggunakan thermometer standar. 5.3.2.

Tabung harus dicuci bersih dengan asam sulfat (1:1), kemudian dibilas dengan air distillat dan dikeringkan.

5.4. Cara Kerja 5.4.1. Set wadah minyak ke suhu 205 + 2 oC dan jaga suhu dalam kisaran khusus ini. 5.4.2. Isi tabung yang bersih dan kering hingga kedalaman 12.7 cm dengan sampel dan masukkan dalam wadah minyak. 5.4.3. Atur volume di dalam wadah minyak hingga ketinggian 14 cm dari bagian bawah gelas tabung. Bila meletakkan beberapa tabung gelas di dalam oil batch, suhunya tidak turun lebih dari 5 oC di bawah suhu minimum oil batch dan waktu untuk menaikkan suhu menjadi 205 oC tidak lebih dari 5 menit. 5.4.4. Atur waktu 60 menit untuk samplel yang memiliki bilangan iodium di atas 15 atau atur 120 menit jika sampel memiliki bilangan iodium lebih kecil atau sama dengan 15. 5.4.5. Pindahkan tabung dari oil batch dan lihat warna menggunakan AOCS official Method Td 1a - 65 atau Lovibond Color.

6. Rujukan AOCS Official Method Td 3a-64

7. Informasi-informasi lain yang dibutuhkan Kebersihan glassware sangat penting. Metode yang disarankan dibersihkan dengan detergent dan dibilas dengan asam sulfat. Larutan dikromat jangan dilakukan.


LAMPIRAN -2A Tabel –L1. Mutu Umpan Hidrogenated Splitted Crude Stearic Acid (HSRBDPSFA).

No

Item Analisa

1

Color 51/4, R/Y

2

Komposisi (% berat):

Bilangan Iodium (IV) Umpan, g / 100 g 0,7 0,6

5,8/44,4

4,9/42,1

Asam laurat, C 12

0,1

0,1

Asam miristat, C 14

1,3

1,3

Asam palmitat, C 16

59,5

56,8

Asam stearat, C 18

38.6

41,3

Asam oleat, C 18-1

-

-

Asam linoleat, C 18-2

-

-

Asam arachidat, C 20

0,4

0,4

Unknown, Unk

0,1

0,1

Sumber : PT. Flora Sawita Chemindo, 2008


LAMPIRAN -2B Tabel –L2. Hasil Perhitungan Nilai Rata-rata Warna Distillat Asam Stearat Berbasis RBDPS.

No

Kecepatan

Bilangan

Alir

Iodium (IV)

Umpan,

Umpan,

ton/jam

g/ 100 g 0,7

1

5,5

0,6

0,7

2

5,75

0,6

0,7

3

6,00

0,6

Warna R DAS Suhu Bottom MD, C0

Warna Y DAS

R R-1

R-2

Rata -

Y Y-1

Y-2

rata

Rata - rata

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

Keterangan : R = Red ; Y = Yellow ; R = harga rata – rata R-1 dan R-2; Y Rata – rata = harga rata – rata Y-1 dan Y-2 sesuai simbol Warna Lovibond


234

LAMPIRAN -2C Tabel –L3. Rata-rata Heat Stability dan Produksi Fraksi Ringan dan Distillat Asam Stearat (DAS) dari RBDPS. Kecepatan No

Alir Umpan, (ton/jam)

Bilangan Iodium (IV) Umpan, g/100 g

0,7 1

0,7

H/S - 2

H/S

LE

DAS

kg/jam

kg/jam

MD, C0

R

Y

R

Y

R

Y

218

0,4

3,8

0,4

4,1

0,40

3,95

82,73

4923,75

220

0,4

4,8

0,5

5,2

0,45

5.00

93,25

4937,25

222

0,5

5,4

0,5

5,8

0,50

5,60

98,55

4967,51

218

0,3

3,7

0.3

3,8

0,30

3,75

95,125

4925,05

220

0,3

4,8

0,4

5,0

0,35

4,90

95,58

4936,85

222

0,4

5,2

0,4

5,3

0,40

5,25

91,40

4949,8

218

0,4

3,9

0,5

4,0

0,45

3,95

86,25

5146,00

220

0,5

4,9

0,5

5,3

0,50

5,10

98,33

5161,50

222

0,6

5,4

0,5

5,8

0,55

5,60

102,93

5194,00

218

0,4

4,0

0,4

3,8

0,40

3,95

99,30

5150,00

220

0,4

4,9

0,5

5,1

0,45

5,00

100,06

5161,25

222

0,5

5,3

0,5

5,4

0,50

5,35

100,65

5196,00

218

0,5

4,0

0,5

4,2

0,50

4,10

90,30

5370,60

220

0,6

5,0

0,6

5,3

0,55

5,15

99,60

5385,90

222

0,6

5,8

0,6

6.0

0,60

5,90

83,70

5435.65

218

0,5

4,0

0,4

4,1

0,45

4,05

103,20

5377,20

220

0,5

4,9

0,5

5,2

0,50

5,05

103,80

5386,30

222

0,6

5,4

0,5

5,5

0,55

5,45

105,30

5444,70

5,75 0,6

0,7 3

H/S – 1

Bottom

5,50 0,6

2

Suhu

6,00 0,6

Keterangan : H/S = heat stability ; R = red ; Y = yellow ; H/S = heat stability rata – rata.


LAMPIRAN -2D Tabel –L4. Hasil Perhitungan Rata - rata Respon Yield Destillat LE, AS dan Residue serta Distillat -2.

Kec. Alir No

Umpan, ton/jam

Yield Fraksi Ringan (LE) IV Umpan, g/ 100 g

0,7

1

5,50

0,6

0,7

2

5,75

0,6

0,7

3

6,00

0,6

Yield Distillat Asam Stearat

Yield Residue

Yield Dist -2

Suhu B MD 0

C

LE-1

LE-2

LE

DAS-1

DAS-2

DAS

Res-1

Res-2

Res

(Dest-2)-1

(Dist-2)-2

Dist-2

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

218

96,750

94,00

95,375

4922,50

4925,,00

4923.75

283,00

285,00

284,00

198,52

196,00

197,26

220

95,150

96,10

95,625

4936,50

4938,00

4937,25

280,00

281,00

280,50

188,85

184,90

186.75

222

99,00

98,00

98,500

4965,015

4970,00

4967,51

277,00

278,00

277,50

158,99

154,00

156,49

218

82,50

83,00

82,750

4924,00

4926,10

4925,05

280,60

277,00

278,80

212,90

214,90

213,90

220

93,50

93,00

93,250

4937,50

4936,20

4936,85

275,50

276,00

275,75

194,00

194,80

194.40

222

95,40

97,10

96,250

4970,50

4969,10

4969,80

274,00

275,00

274,50

160,10

158,80

159,45

218

100,80

97,80

99,300

5143,40

5148,60

5146,00

297,30

299,40

298,35

208,50

204,20

206,35

220

99,48

100,63

100,055

5161,20

5161,80

5161,50

292,67

293,00

292,835

196,65

194,57

195,70

222

102,35

103,50

102,925

5192,30

5195,70

5194,00

287,50

289,80

288,50

167,85

161,00

164,425

218

85,70

86,80

86,250

5148,00

5152,00

5150,00

293,30

291,50

292,40

223,00

219,70

221,35

220

94,88

97,17

96,025

5161,78

5160,63

5161,25

288,50

288,80

288,65

204,84

203,40

204,12

222

100,10

101,20

110,150

5196,30

5195,70

5196,00

284,05

286,35

285,20

169,55

166,75

168,15

218

105,00

101,40

103,200

5368,20

5373,00

5370,60

308,00

309,00

308,50

218,80

216,60

217,70

220

103,20

104,44

103,800

5385,60

5386,20

5385,90

304,20

305,40

304,80

207,80

204,00

205,90

222

107,40

109,20

108,300

5435,10

5436,20

5435.65

301,20

302,40

301,80

156,30

152,20

154,25

218

90,15

90,60

90,375

5372,40

5382,00

5377,20

303,00

302,5

302,75

234,60

225,40

230,00

220

98,40

100,80

99,600

5385,00

5388,00

5386,30

300,60

301,80

301,20

216,00

209,40

212,70

222

104,40

106,20

105,300

5444,20

5445,20

5444,70

297,00

298,20

297,60

152,60

152,20

152,40


LAMPIRAN -2E Tabel –L5. Hasil Perhitungan Rata-rata Bilangan Iodium (IV) Distillat Asam Stearat Berbasis RBDPS. Kecepatan No

Alir Umpan, ton/jam

Bilangan Iodium (IV) Umpan, g/ 100 g 0,7

1

5,5 0,6

0,7 2

5,75 0,6

0,7 3

6,00 0,6

Bilangan Iodium (IV) DAS

Suhu

IV Rata -

Bottom MD,

IV– 1

IV – 2

C0

gr/100 gr

gr/100 gr

218

0.15

0,15

0.150

220

0.15

0,17

0.160

222

0,17

0,17

0,170

218

0.14

0,15

0.145

220

0,16

0.15

0.155

222

0,16

0.16

0.160

218

0.16

0,16

0.160

220

0,17

0,17

0,170

222

0,17

0,17

0,170

218

0,16

0,15

0.155

220

0.16

0,17

0.165

222

0,17

0.16

0.165

218

0,16

0.17

0.165

220

0.18

0,17

0.175

222

0,18

0,18

0,180

218

0,16

0.16

0,160

220

0,17

0.17

0,170

222

0,18

0.17

0.175

rata gr/100 gr


LAMPIRAN -2F Tabel –L6. Hasil Perhitungan Rata - Rata Bilangan Asam Residue Berbasis RBDPS. Kecepatan Alir No

Umpan, ton/jam

Bilangan Iodium (IV) Umpan, 100 g

0,7 1

5,5 0,6

0,7 2

5,75 0,6

0,7 3

6,00 0,6

g/

Bilangan Asam (AV) Residue

Suhu Bottom MD,

AV – 1,

AV – 2,

AV Rata - rata,

218

33,5

36,5

35,00

220

25,8

28,0

26,90

222

25,5

27,5

26,50

218

28,3

27,8

28,05

220

23,9

24,5

24,20

222

23,6

25,1

24,30

218

33,6

36,4

35,00

220

26,0

27,6

26,80

222

25,0

27,5

26,25

218

28,5

27,8

28,15

220

24,5

24,8

24,65

222

24,0

24,8

24,40

218

34,0

37,0

35,50

220

26,5

27,5

27,00

222

25,8

27,8

26,80

218

28,2

28,0

28,10

220

25,0

24.5

24.75

222

23,80

24,6

24,20

C0

Keterangan : AV = Acid Value (Bilangan Asam) dalam mg KOH/gram


LAMPIRAN -2G Tabel –L7. Perbandingan Mutu Distillat Asam Stearat (berbasis RBDPS) Hasil Optimasi Mutu DAS Sebelum Optimasi (*) 0,10,2R/0,70,9Y

Mutu DAS Sesudah Optimasi

0,5-0,8R/67,5Y

0,55R/5,45 Y

0,15 - 0,24

0,175

total keduanya 1,0 % maks

< 1,0


C 16 , asam palmitat

56 - 63

In specs

59,00

C 18 , asam stearat

37 – 42

Sering < 37.0

40,25

< 1,0

total keduanya 0,45 %

No

Parameter Mutu

1

Warna (Colour) 5 ¼ “, Lovibond

2

Heat Stability (H/S)5 ¼”, Lovibond

3

Bilangan Iodium (IV), gr/100 gr

4

Komposisi, % berat : C 12 , asam laurat C 14 , asam miristat

C 20 , asam arachidat Unk

Standar Mutu DAS 0,1R/ 0,8Y maks 0,6 R/6,0Y maks 0,20 maks


0.1/0.7


LAMPIRAN 3A General Linear Model: Yield AS versus F Umpan, IV Umpan, Suhu B MD Factor F Umpan IV Umpan Suhu B MD

Type fixed fixed fixed

Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for Yield AS, using Adjusted SS for Tests Source P F Umpan 0.000 IV Umpan 0.004 Suhu B MD 0.000 F Umpan*IV Umpan 0.105 F Umpan*Suhu B MD 0.000 IV Umpan*Suhu B MD 0.081 F Umpan*IV Umpan*Suhu B MD 0.681 Error Total

S = 2.49864

R-Sq = 99.99%

DF

Seq SS

Adj SS

Adj MS

F

2

1251684

1251684

625842

100243.94

1

70

70

70

11.25

2

17999

17999

9000

1441.52

2

32

32

16

2.56

4

793

793

198

31.74

2

36

36

18

2.90

4

14

14

4

0.58

18 35

112 1270741

112

6

R-Sq(adj) = 99.98%

Unusual Observations for Yield AS Obs 31 32

Yield AS 5372.40 5382.00

Fit 5377.20 5377.20

SE Fit 1.77 1.77

Residual -4.80 4.80

St Resid -2.72 R 2.72 R

R denotes an observation with a large standardized residual.


LAMPIRAN -3B One-way ANOVA: Yield AS_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total S = 25.65

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 631841 9870 641711

MS 315920 658

R-Sq = 98.46%

Mean 4943.9 5169.1 5402.8

StDev 20.8 21.5 32.9

F 480.10

P 0.000

R-Sq(adj) = 98.26%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(-*) (-*) (*-) --+---------+---------+---------+------4950 5100 5250 5400

Pooled StDev = 25.7

Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of F Umpan_0.6 Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from: F Umpan_0.6 5.75 6.00

Lower 193.60 427.33

Center 225.17 458.90

Upper 256.74 490.47

---+---------+---------+---------+-----(*-) (-*-) ---+---------+---------+---------+------200 0 200 400

F Umpan_0.6 = 5.75 subtracted from: F Umpan_0.6 6.00

Lower 202.16

Center 233.73

Upper 265.30

---+---------+---------+---------+-----(-*) ---+---------+---------+---------+------200 0 200 400


LAMPIRAN -3C MTB > Oneway 'Yield AS_0.7' 'F Umpan_0.7'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total S = 24.61

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 619875 9085 628960

MS 309937 606

R-Sq = 98.56%

Mean 4942.8 5167.2 5397.4

StDev 20.1 22.0 30.5

F 511.75

P 0.000

R-Sq(adj) = 98.36%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(-*) (*-) (-*) --+---------+---------+---------+------4950 5100 5250 5400

Pooled StDev = 24.6


F Umpan_0.7 = 5.50 subtracted from: F Umpan_0.7 ---5.75 6.00 *)

Lower

Center

Upper

194.05 424.26

224.33 454.55

254.62 484.83

---+---------+---------+---------+-(*-) (---+---------+---------+---------+--

----200

0

200

400

F Umpan_0.7 = 5.75 subtracted from: F Umpan_0.7 ---6.00

Lower

Center

Upper

199.93

230.21

260.50

---+---------+---------+---------+-(-*)


---+---------+---------+---------+-----200

0

200

400

LAMPIRAN -3D One-way ANOVA: Yield AS_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total S = 20.45

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 3 4181 4184

MS 3 418

R-Sq = 0.08%

Mean 4943.9 4942.8

StDev 20.8 20.1

F 0.01

P 0.930

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(------------------*-----------------) (------------------*-----------------) ------+---------+---------+---------+--4930 4940 4950 4960

Pooled StDev = 20.4

Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of IV Umpan_5.50 Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from: IV Umpan_5.50 ---+0.7 )

Lower

Center

Upper

--------+---------+---------+------

-27.37

-1.06

25.24

(----------------*------------------------+---------+---------+------

---+-15

0

15

30


LAMPIRAN -3E One-way ANOVA: Yield AS_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total S = 21.75

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 11 4731 4741

R-Sq = 0.23%

Mean 5169.1 5167.2

StDev 21.5 22.0

MS 11 473

F 0.02

P 0.883

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(----------------*---------------) (----------------*---------------) -+---------+---------+---------+-------5148 5160 5172 5184

Pooled StDev = 21.8


IV Umpan_5.75 = 0.6 subtracted from: IV Umpan_5.75 0.7

Lower -29.88

Center -1.90

Upper 26.08

IV Umpan_5.75 0.7

+---------+---------+---------+--------(------------------*-----------------) +---------+---------+---------+---------30 -15 0 15

MTB > Oneway 'Yield AS_6.00' 'IV Umpan_6.00'; SUBC> Fisher 5.


LAMPIRAN -3F One-way ANOVA: Yield AS_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total S = 31.69

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 88 10044 10132

R-Sq = 0.87%

Mean 5402.8 5397.4

StDev 32.9 30.5

MS 88 1004

F 0.09

P 0.773

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(-----------------*-----------------) (-----------------*-----------------) -----+---------+---------+---------+---5376 5392 5408 5424

Pooled StDev = 31.7


IV Umpan_6.00 = 0.6 subtracted from: IV Umpan_6.00 ---+0.7

Lower

Center

Upper

--------+---------+---------+------

-46.19

-5.42

35.35

(---------------*---------------) --------+---------+---------+------

---+-25

0

25

50


LAMPIRAN -3G MTB > Oneway 'Yield AS_218' 'F Umpan_218'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_218 versus F Umpan_218 Source F Umpan_218 Error Total S = 4.024

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 404104.0 145.7 404249.7

MS 202052.0 16.2

R-Sq = 99.96%

Mean 4924.40 5148.00 5373.90

StDev 1.53 3.54 5.81

F 12480.91

P 0.000

R-Sq(adj) = 99.96%

Individual 95% CIs For Mean Based on Pooled StDev +---------+---------+---------+--------*) * (* +---------+---------+---------+--------4920 5040 5160 5280

Pooled StDev = 4.02

Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of F Umpan_218 Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from: F Umpan_218 ----5.75 6.00 *)

Lower

Center

Upper

217.16 443.06

223.60 449.50

230.04 455.94

--+---------+---------+---------+-*)

--+---------+---------+---------+------200

0

200

400

F Umpan_218 = 5.75 subtracted from: F Umpan_218 ----6.00

Lower

Center

Upper

--+---------+---------+---------+--

219.46

225.90

232.34

*) --+---------+---------+---------+--

-----200

0

200

400


LAMPIRAN -3H MTB > Oneway 'Yield AS_220' 'F Umpan_220'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_220 versus F Umpan_220 Source F Umpan_220 Error Total

DF 2 9 11

S = 0.9486

R-Sq = 100.00%

Level 5.50 5.75 6.00

N 4 4 4

SS 403471.6 8.1 403479.7

Mean 4937.05 5161.35 5386.20

StDev 0.84 0.56 1.30

MS 201735.8 0.9

F 224198.66

P 0.000

R-Sq(adj) = 100.00%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ *) * * ---------+---------+---------+---------+ 5040 5160 5280 5400

Pooled StDev = 0.95


F Umpan_220 = 5.50 subtracted from: F Umpan_220 5.75 6.00

Lower 222.785 447.633

Center 224.303 449.150

Upper 225.820 450.667

F Umpan_220 5.75 6.00

-+---------+---------+---------+-------* *) -+---------+---------+---------+--------200 0 200 400

F Umpan_220 = 5.75 subtracted from: F Umpan_220 6.00

Lower 223.330

Center 224.847

Upper 226.365

F Umpan_220 6.00

-+---------+---------+---------+-------* -+---------+---------+---------+--------200 0 200 400


LAMPIRAN -3I MTB > Oneway 'Yield AS_222' 'F Umpan_222'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_222 versus F Umpan_222 Source F Umpan_222 Error Total S = 3.521

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 444900.8 111.6 445012.4

MS 222450.4 12.4

R-Sq = 99.97%

Mean 4968.65 5195.00 5440.18

StDev 2.49 1.82 5.26

F 17943.69

P 0.000

R-Sq(adj) = 99.97%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--* * *) ------+---------+---------+---------+--5040 5160 5280 5400

Pooled StDev = 3.52


F Umpan_222 = 5.50 subtracted from: F Umpan_222 ---5.75 6.00 (*

Lower

Center

Upper

220.72 465.89

226.35 471.52

231.98 477.15

---+---------+---------+---------+-*)

---+---------+---------+---------+-----200

0

200

400

F Umpan_222 = 5.75 subtracted from: F Umpan_222 ---6.00

Lower

Center

Upper

---+---------+---------+---------+--

239.54

245.17

250.80

*) ---+---------+---------+---------+--

----200

0

200

400


LAMPIRAN -3J Results for: Worksheet 3 MTB > Oneway 'Yield AS_5.50' 'Suhu B MD_5.50'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_5.50 versus Suhu B MD_5.50 Source Suhu B MD_5.50 Error Total S = 1.758

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 4156.29 27.81 4184.10

R-Sq = 99.34%

Mean 4924.40 4937.05 4968.65

StDev 1.53 0.84 2.49

MS 2078.14 3.09

F 672.52

P 0.000

R-Sq(adj) = 99.19%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(*) (*-) (*-) --------+---------+---------+---------+4935 4950 4965 4980

Pooled StDev = 1.76

Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of Suhu B MD_5.50 Simultaneous confidence level = 88.66%

Suhu B MD_5.50 = 218 subtracted from: Suhu B MD_5.50 220 222

Lower 9.838 41.442

Center 12.650 44.254

Upper 15.462 47.066

----+---------+---------+---------+----(*) (*) ----+---------+---------+---------+-----25 0 25 50

Suhu B MD_5.50 = 220 subtracted from: Suhu B MD_5.50 222

Lower 28.792

Center 31.604

Upper 34.416

----+---------+---------+---------+----(*) ----+---------+---------+---------+-----25 0 25 50


LAMPIRAN -3K MTB > Oneway 'Yield AS_5.75' 'Suhu B MD_5.75'; SUBC> Fisher 5.


Level 218 220 222

N 4 4 4

DF 2 9 11

SS 4693.13 48.35 4741.48

R-Sq = 98.98%

Mean 5148.00 5161.35 5195.00

StDev 3.54 0.56 1.82

MS 2346.56 5.37

F 436.76

P 0.000

R-Sq(adj) = 98.75%

Individual 95% CIs For Mean Based on Pooled StDev +---------+---------+---------+--------(-*-) (-*-) (*-) +---------+---------+---------+--------5145 5160 5175 5190

Pooled StDev = 2.32



Lower 9.645 43.295

Center 13.352 47.003

Upper 17.060 50.710

-----+---------+---------+---------+---(*-) (-*) -----+---------+---------+---------+----25 0 25 50


Lower 29.942

Center 33.650

Upper 37.358

-----+---------+---------+---------+---(*-) -----+---------+---------+---------+----25 0 25 50


LAMPIRAN -3L MTB > Oneway 'Yield AS_6.00' 'Suhu B MD_6.00'; SUBC> Fisher 5.


Level 218 220 222

N 4 4 4

DF 2 9 11

SS 9942.6 189.2 10131.8

R-Sq = 98.13%

Mean 5373.90 5386.20 5440.18

StDev 5.81 1.30 5.26

MS 4971.3 21.0

F 236.47

P 0.000

R-Sq(adj) = 97.72%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--*--) (-*--) (--*--) ------+---------+---------+---------+--5380 5400 5420 5440

Pooled StDev = 4.59



Lower 4.966 58.941

Center 12.300 66.275

Upper 19.634 73.609

--------+---------+---------+---------+(--*-) (-*-) --------+---------+---------+---------+-35 0 35 70


Lower 46.641

Center 53.975

Upper 61.309

--------+---------+---------+---------+(-*--) --------+---------+---------+---------+-35 0 35 70


LAMPIRAN -3M Results for: Worksheet 2 MTB > Oneway 'Yield AS_0.6' 'Suhu B MD_0.6'; SUBC> Fisher 5.


Level 218 220 222

N 6 6 6

DF 2 15 17

SS 9322 632389 641711

R-Sq = 1.45%

Mean 5150.8 5161.5 5203.5

StDev 202.2 201.1 212.5

MS 4661 42159

F 0.11

P 0.896

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--------------*--------------) (--------------*--------------) (--------------*--------------) ------+---------+---------+---------+--5040 5160 5280 5400

Pooled StDev = 205.3



Lower -241.9 -199.9

Center 10.8 52.8

Upper 263.4 305.4

--------+---------+---------+---------+(---------------*--------------) (--------------*---------------) --------+---------+---------+---------+-160 0 160 320


Lower -210.7

Center 42.0

Upper 294.7

--------+---------+---------+---------+(---------------*--------------)


--------+---------+---------+---------+-160 0 160 320

LAMPIRAN -3N MTB > Oneway 'Yield AS_0.7' 'Suhu B MD_0.7'; SUBC> Fisher 5.


Level 218 220 222

N 6 6 6

DF 2 15 17

SS 8714 620246 628960

R-Sq = 1.39%

Mean 5146.8 5161.6 5199.1

StDev 199.9 200.6 209.4

MS 4357 41350

F 0.11

P 0.901

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--------------*--------------) (--------------*--------------) (-------------*--------------) ------+---------+---------+---------+--5040 5160 5280 5400




Lower -235.5 -198.0

Center 14.8 52.3

Upper 265.0 302.5

---------+---------+---------+---------+ (----------------*----------------) (---------------*----------------) ---------+---------+---------+---------+ -150 0 150 300


Lower -212.7

Center 37.5

Upper 287.7

---------+---------+---------+---------+ (----------------*---------------)


---------+---------+---------+---------+ -150 0 150 300

LAMPIRAN -3O Results for: Worksheet 5 MTB > Oneway 'Yield AS_218' 'IV Umpan_218'; SUBC> Fisher 5.

One-way ANOVA: Yield AS_218 versus IV Umpan_218 Source IV Umpan_218 Error Total S = 201.0

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 47 404203 404250

R-Sq = 0.01%

Mean 5150.8 5146.8

StDev 202.2 199.9

MS 47 40420

F 0.00

P 0.973

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(-----------------*-----------------) (------------------*-----------------) ----+---------+---------+---------+----5000 5100 5200 5300


Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of IV Umpan_218 Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from: IV Umpan_218 --+0.7

Lower

Center

Upper

--------+---------+---------+-------

-262.6

-4.0

254.7

(-----------------*----------------) --------+---------+---------+-------

--+-150

0

150

300


LAMPIRAN -3P MTB > Oneway 'Yield AS_220' 'IV Umpan_220'; SUBC> Fisher 5.


Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0 403480 403480

R-Sq = 0.00%

Mean 5161.5 5161.6

StDev 201.1 200.6

MS 0 40348

F 0.00

P 1.000

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(-----------------*-----------------) (-----------------*-----------------) --+---------+---------+---------+------5000 5100 5200 5300



IV Umpan_220 = 0.6 subtracted from: IV Umpan_220 -+-0.7

Lower

Center

Upper

-------+---------+---------+--------

-258.4

0.0

258.4

(----------------*----------------) -------+---------+---------+--------

-+--150

0

150

300


LAMPIRAN -3Q MTB > Oneway 'Yield AS_222' 'IV Umpan_222'; SUBC> Fisher 5.


Level 0.6 0.7

N 6 6

DF 1 10 11

SS 59 444953 445012

R-Sq = 0.01%

Mean 5203.5 5199.1

StDev 212.5 209.4

MS 59 44495

F 0.00

P 0.972

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (------------------*-------------------) (------------------*------------------) ---------+---------+---------+---------+ 5100 5200 5300 5400



IV Umpan_222 = 0.6 subtracted from: IV Umpan_222 --+0.7 )

Lower

Center

Upper

--------+---------+---------+-------

-275.8

-4.4

266.9

(-----------------*-----------------


--------+---------+---------+--------+-150

0

150

300 MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.26"; SUBC> Project; SUBC> Replace.

————— 5/10/2009 5:57:13 PM ———————————————————

LAMPIRAN -4A ————— 7/13/2009 9:33:10 PM ——————————————————— Welcome to Minitab, press F1 for help.

General Linear Model: IV DAS versus F Umpan, IV Umpan, Suhu B MD Factor F Umpan IV Umpan Suhu B MD


Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for IV DAS, using Adjusted SS for Tests Source P F Umpan 0.000 IV Umpan 0.010 Suhu B MD 0.000 F Umpan*IV Umpan 0.920 F Umpan*Suhu B MD 0.679 IV Umpan*Suhu B MD 0.920 F Umpan*IV Umpan*Suhu B MD 0.986 Error Total

DF

Seq SS

Adj SS

Adj MS

F

2

0.0012056

0.0012056

0.0006028

18.08

1

0.0002778

0.0002778

0.0002778

8.33

2

0.0012722

0.0012722

0.0006361

19.08

2

0.0000056

0.0000056

0.0000028

0.08

4

0.0000778

0.0000778

0.0000194

0.58

2

0.0000056

0.0000056

0.0000028

0.08

4

0.0000111

0.0000111

0.0000028

0.08

18 35

0.0006000 0.0034556

0.0006000

0.0000333


S = 0.00577350

R-Sq = 82.64%

R-Sq(adj) = 66.24%

LAMPIRAN -4B Results for: Worksheet 2 One-way ANOVA: IV DAS_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total S = 0.007746

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.0006778 0.0009000 0.0015778

MS 0.0003389 0.0000600

R-Sq = 42.96%

Mean 0.15333 0.16167 0.16833

StDev 0.00816 0.00753 0.00753

F 5.65

P 0.015

R-Sq(adj) = 35.35%

Individual 95% CIs For Mean Based on Pooled StDev -------+---------+---------+---------+-(--------*-------) (-------*--------) (-------*--------) -------+---------+---------+---------+-0.1520 0.1600 0.1680 0.1760





Lower -0.001199 0.005468

Center 0.008333 0.015000

Upper 0.017865 0.024532

F Umpan_0.6 5.75 6.00

---+---------+---------+---------+-----(-------*-------) (------*-------) ---+---------+---------+---------+------0.012 0.000 0.012 0.024


Lower -0.002865

F Umpan_0.6 6.00

---+---------+---------+---------+-----(-------*------) ---+---------+---------+---------+------0.012 0.000 0.012 0.024

Center 0.006667

Upper 0.016199

LAMPIRAN -4C One-way ANOVA: IV DAS_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total S = 0.008433

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.0005333 0.0010667 0.0016000

MS 0.0002667 0.0000711

R-Sq = 33.33%

Mean 0.16000 0.16667 0.17333

StDev 0.01095 0.00516 0.00816

F 3.75

P 0.048

R-Sq(adj) = 24.44%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (--------*--------) (--------*---------) (---------*--------) ---------+---------+---------+---------+ 0.1600 0.1680 0.1760 0.1840





Lower -0.003711 0.002956

Center 0.006667 0.013333

Upper 0.017044 0.023711

F Umpan_0.7 5.75 6.00

----+---------+---------+---------+----(--------*-------) (--------*--------) ----+---------+---------+---------+-----0.012 0.000 0.012 0.024


Lower -0.003711

Center 0.006667

Upper 0.017044

F Umpan_0.7 6.00

----+---------+---------+---------+----(--------*-------) ----+---------+---------+---------+-----0.012 0.000 0.012 0.024

LAMPIRAN -4D Results for: Worksheet 4 One-way ANOVA: IV DAS_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total

DF 1 10 11

S = 0.009661

R-Sq = 12.50%

Level 0.6 0.7

N 6 6

Mean 0.15333 0.16000

SS 0.0001333 0.0009333 0.0010667

StDev 0.00816 0.01095

MS 0.0001333 0.0000933

F 1.43

P 0.260

R-Sq(adj) = 3.75%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(------------*------------) (------------*-----------) ----+---------+---------+---------+----0.1470 0.1540 0.1610 0.1680


Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of IV Umpan_5.50


Simultaneous confidence level = 95.00%


Lower -0.005761

Center 0.006667

Upper 0.019095

IV Umpan_5.50 0.7

------+---------+---------+---------+--(--------------*---------------) ------+---------+---------+---------+---0.0080 0.0000 0.0080 0.0160

LAMPIRAN -4E One-way ANOVA: IV DAS_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total

DF 1 10 11

S = 0.006455

R-Sq = 15.25%

Level 0.6 0.7

N 6 6

Mean 0.16167 0.16667

SS 0.0000750 0.0004167 0.0004917

StDev 0.00753 0.00516

MS 0.0000750 0.0000417

F 1.80

P 0.209

R-Sq(adj) = 6.78%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(----------*-----------) (----------*-----------) --------+---------+---------+---------+0.1600 0.1650 0.1700 0.1750






Lower -0.003304

Center 0.005000

Upper 0.013304

IV Umpan_5.75 0.7

----+---------+---------+---------+----(-------------*-------------) ----+---------+---------+---------+-----0.0060 0.0000 0.0060 0.0120

LAMPIRAN -4F One-way ANOVA: IV DAS_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total

DF 1 10 11

S = 0.007853

R-Sq = 10.84%

Level 0.6 0.7

N 6 6

Mean 0.16833 0.17333

SS 0.0000750 0.0006167 0.0006917

StDev 0.00753 0.00816

MS 0.0000750 0.0000617

F 1.22

P 0.296

R-Sq(adj) = 1.93%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(--------------*-------------) (--------------*-------------) --------+---------+---------+---------+0.1650 0.1700 0.1750 0.1800


Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00 Simultaneous confidence level = 95.00%


Lower -0.005102

Center 0.005000

Upper 0.015102

IV Umpan_6.00 0.7

----+---------+---------+---------+----(-------------*--------------) ----+---------+---------+---------+-----0.0070 0.0000 0.0070 0.0140

LAMPIRAN -4G Results for: Worksheet 3 One-way ANOVA: IV DAS_218 versus F Umpan_218 Source F Umpan_218 Error Total S = 0.005

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.0004667 0.0002250 0.0006917

R-Sq = 67.47%

Mean 0.14750 0.15750 0.16250

StDev 0.00500 0.00500 0.00500

MS 0.0002333 0.0000250

F 9.33

P 0.006

R-Sq(adj) = 60.24%

Individual 95% CIs For Mean Based on Pooled StDev -------+---------+---------+---------+-(-------*-------) (-------*-------) (-------*-------) -------+---------+---------+---------+-0.1470 0.1540 0.1610 0.1680





Lower 0.002002 0.007002

Center 0.010000 0.015000

Upper 0.017998 0.022998

F Umpan_218 5.75 6.00

---+---------+---------+---------+-----(-------*-------) (-------*-------) ---+---------+---------+---------+------0.010 0.000 0.010 0.020


Lower -0.002998

F Umpan_218 6.00

---+---------+---------+---------+-----(-------*-------) ---+---------+---------+---------+------0.010 0.000 0.010 0.020

Center 0.005000

Upper 0.012998

LAMPIRAN -4H One-way ANOVA: IV DAS_220 versus F Umpan_220 Source F Umpan_220 Error Total S = 0.006872

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.0004667 0.0004250 0.0008917

MS 0.0002333 0.0000472

R-Sq = 52.34%

Mean 0.15750 0.16750 0.17250

StDev 0.00957 0.00500 0.00500

F 4.94

P 0.036

R-Sq(adj) = 41.74%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(---------*---------) (--------*---------) (---------*--------) ---+---------+---------+---------+-----0.1520 0.1600 0.1680 0.1760





Lower -0.000992 0.004008

Center 0.010000 0.015000

Upper 0.020992 0.025992

F Umpan_220 5.75 6.00

---+---------+---------+---------+-----(--------*--------) (---------*--------) ---+---------+---------+---------+------0.012 0.000 0.012 0.024


Lower -0.005992

Center 0.005000

F Umpan_220 6.00

---+---------+---------+---------+-----(--------*--------) ---+---------+---------+---------+------0.012 0.000 0.012 0.024

Upper 0.015992

LAMPIRAN -4I One-way ANOVA: IV DAS_222 versus F Umpan_222 Source F Umpan_222 Error Total S = 0.005270

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.0003500 0.0002500 0.0006000

MS 0.0001750 0.0000278

R-Sq = 58.33%

Mean 0.16500 0.16750 0.17750

StDev 0.00577 0.00500 0.00500

F 6.30

P 0.019

R-Sq(adj) = 49.07%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(--------*-------) (-------*--------) (--------*-------) ---+---------+---------+---------+------


0.1610

0.1680

0.1750

0.1820




Lower -0.005931 0.004069

Center 0.002500 0.012500

Upper 0.010931 0.020931

F Umpan_222 5.75 6.00

--------+---------+---------+---------+(--------*-------) (-------*--------) --------+---------+---------+---------+-0.010 0.000 0.010 0.020


Lower 0.001569

Center 0.010000

Upper 0.018431

F Umpan_222 6.00

--------+---------+---------+---------+(-------*-------) --------+---------+---------+---------+-0.010 0.000 0.010 0.020

LAMPIRAN -4J Results for: Worksheet 4 One-way ANOVA: IV DAS_5.50 versus Suhu B MD_5.50 Source Suhu B MD_5.50 Error Total S = 0.007071

DF 2 9 11

SS 0.0006167 0.0004500 0.0010667

R-Sq = 57.81%

MS 0.0003083 0.0000500

F 6.17

P 0.021

R-Sq(adj) = 48.44%

Individual 95% CIs For Mean Based on Pooled StDev


Level 218 220 222

N 4 4 4

Mean 0.14750 0.15750 0.16500

StDev 0.00500 0.00957 0.00577

+---------+---------+---------+--------(------*-------) (------*-------) (-------*-------) +---------+---------+---------+--------0.140 0.150 0.160 0.170



Suhu B MD_5.50 = 218 subtracted from: Suhu B MD_5.50 220 222 Suhu B MD_5.50 220 222

Lower -0.001311 0.006189

Center 0.010000 0.017500

Upper 0.021311 0.028811

------+---------+---------+---------+--(--------*---------) (---------*--------) ------+---------+---------+---------+---0.012 0.000 0.012 0.024

Suhu B MD_5.50 = 220 subtracted from: Suhu B MD_5.50 222 Suhu B MD_5.50 222

Lower -0.003811

Center 0.007500

Upper 0.018811

------+---------+---------+---------+--(--------*---------) ------+---------+---------+---------+---0.012 0.000 0.012 0.024

LAMPIRAN -4K One-way ANOVA: IV DAS_5.75 versus Suhu B MD_5.75 Source Suhu B MD_5.75 Error Total S = 0.005

DF 2 9 11

SS 0.0002667 0.0002250 0.0004917

R-Sq = 54.24%

MS 0.0001333 0.0000250

F 5.33

P 0.030

R-Sq(adj) = 44.07%

Individual 95% CIs For Mean Based on Pooled StDev


Level 218 220 222

N 4 4 4

Mean 0.15750 0.16750 0.16750

StDev 0.00500 0.00500 0.00500

-------+---------+---------+---------+-(---------*--------) (--------*---------) (--------*---------) -------+---------+---------+---------+-0.1560 0.1620 0.1680 0.1740



Suhu B MD_5.75 = 218 subtracted from: Suhu B MD_5.75 220 222 Suhu B MD_5.75 220 222

Lower 0.002002 0.002002

Center 0.010000 0.010000

Upper 0.017998 0.017998

-+---------+---------+---------+-------(----------*-----------) (----------*-----------) -+---------+---------+---------+--------0.0070 0.0000 0.0070 0.0140


Lower -0.007998

Center 0.000000

Upper 0.007998

-+---------+---------+---------+-------(----------*----------) -+---------+---------+---------+--------0.0070 0.0000 0.0070 0.0140

LAMPIRAN -4L One-way ANOVA: IV DAS_6.00 versus Suhu B MD_6.00 Source Suhu B MD_6.00 Error Total S = 0.005

DF 2 9 11

SS 0.0004667 0.0002250 0.0006917

R-Sq = 67.47%

MS 0.0002333 0.0000250

F 9.33

P 0.006

R-Sq(adj) = 60.24%


Level 218 220 222

N 4 4 4

Mean 0.16250 0.17250 0.17750

StDev 0.00500 0.00500 0.00500

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(-------*-------) (-------*--------) (--------*-------) ------+---------+---------+---------+--0.1610 0.1680 0.1750 0.1820



Suhu B MD_6.00 = 218 subtracted from: Suhu B MD_6.00 +-----220 222 --)

Lower

Center

Upper

0.002002 0.007002

0.010000 0.015000

0.017998 0.022998

---+---------+---------+--------(-------*-------) (-------*-------+---------+---------+---------

+------0.010

0.000

0.010

0.020


Lower -0.002998

Center 0.005000

Upper 0.012998

---+---------+---------+---------+-----(-------*-------) ---+---------+---------+---------+------0.010 0.000 0.010 0.020

LAMPIRAN -4M Results for: Worksheet 2 One-way ANOVA: IV DAS_0.6 versus Suhu B MD_0.6 Source

DF

SS

MS

F

P


Suhu B MD_0.6 Error Total

2 15 17

S = 0.008165

R-Sq = 36.62%

Level 218 220 222

N 6 6 6

Mean 0.15333 0.16333 0.16667

0.0005778 0.0010000 0.0015778

StDev 0.00816 0.00816 0.00816

0.0002889 0.0000667

4.33

0.033

R-Sq(adj) = 28.17%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(---------*---------) (---------*---------) (---------*---------) -+---------+---------+---------+-------0.1470 0.1540 0.1610 0.1680



Suhu B MD_0.6 = 218 subtracted from: Suhu B MD_0.6 Lower +-----220 -0.000048 222 0.003286 --)

Center

Upper

0.010000 0.013333

0.020048 0.023381

---+---------+---------+--------(---------*---------) (---------*---------+---------+---------+---------

+------0.010

0.000

0.010

0.020

Suhu B MD_0.6 = 220 subtracted from: Suhu B MD_0.6 Lower +-----222 -0.006714

Center

Upper

---+---------+---------+---------

0.003333

0.013381

(---------*---------) ---+---------+---------+---------

+------0.010

0.000

0.010

0.020

LAMPIRAN -4N One-way ANOVA: IV DAS_0.7 versus Suhu B MD_0.7


Source Suhu B MD_0.7 Error Total

DF 2 15 17

S = 0.007746

R-Sq = 43.75%

Level 218 220 222

N 6 6 6

Mean 0.15833 0.16833 0.17333

SS 0.0007000 0.0009000 0.0016000

StDev 0.00753 0.00983 0.00516

MS 0.0003500 0.0000600

F 5.83

P 0.013

R-Sq(adj) = 36.25%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(--------*-------) (-------*--------) (--------*-------) -+---------+---------+---------+-------0.1520 0.1600 0.1680 0.1760



Suhu B MD_0.7 = 218 subtracted from: Suhu B MD_0.7 +---220 ) 222 -----)

Lower

Center

Upper

-----+---------+---------+---------

0.000468

0.010000

0.019532

(---------*---------

0.005468

0.015000

0.024532

(---------*--------+---------+---------+---------

+----0.010

0.000

0.010

0.020

Suhu B MD_0.7 = 220 subtracted from: Suhu B MD_0.7 -+---222

Lower

Center

Upper

-----+---------+---------+--------

-0.004532

0.005000

0.014532

(---------*---------) -----+---------+---------+--------

-+----0.010

0.000

0.010

0.020


LAMPIRAN -4O Results for: Worksheet 3 One-way ANOVA: IV DAS_218 versus IV Umpan_218 Source IV Umpan_218 Error Total S = 0.007853

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.0000750 0.0006167 0.0006917

MS 0.0000750 0.0000617

R-Sq = 10.84%

Mean 0.15333 0.15833

StDev 0.00816 0.00753

F 1.22

P 0.296

R-Sq(adj) = 1.93%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(--------------*-------------) (--------------*-------------) --------+---------+---------+---------+0.1500 0.1550 0.1600 0.1650



IV Umpan_218 = 0.6 subtracted from: IV Umpan_218 0.7

Lower -0.005102

Center 0.005000

Upper 0.015102

IV Umpan_218 0.7

----+---------+---------+---------+----(-------------*--------------) ----+---------+---------+---------+-----0.0070 0.0000 0.0070 0.0140


LAMPIRAN -4P One-way ANOVA: IV DAS_220 versus IV Umpan_220 Source IV Umpan_220 Error Total S = 0.009037

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.0000750 0.0008167 0.0008917

R-Sq = 8.41%

Mean 0.16333 0.16833

StDev 0.00816 0.00983

MS 0.0000750 0.0000817

F 0.92

P 0.360

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(------------*-------------) (-------------*------------) -+---------+---------+---------+-------0.1560 0.1620 0.1680 0.1740




Lower -0.006625

Center 0.005000

IV Umpan_220 0.7

-----+---------+---------+---------+---(-------------*--------------) -----+---------+---------+---------+----0.0080 0.0000 0.0080 0.0160

Upper 0.016625


LAMPIRAN -4Q One-way ANOVA: IV DAS_222 versus IV Umpan_222 Source IV Umpan_222 Error Total S = 0.006831

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.0001333 0.0004667 0.0006000

MS 0.0001333 0.0000467

R-Sq = 22.22%

Mean 0.16667 0.17333

StDev 0.00816 0.00516

F 2.86

P 0.122

R-Sq(adj) = 14.44%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (-----------*------------) (------------*-----------) ---------+---------+---------+---------+ 0.1650 0.1700 0.1750 0.1800




Lower -0.002121

Center 0.006667

Upper 0.015455

IV Umpan_222 0.7

---+---------+---------+---------+-----(------------*-----------) ---+---------+---------+---------+------0.0070 0.0000 0.0070 0.0140

————— 7/14/2009 5:49:26 AM ———————————————————


LAMPIRAN – 5A ————— 7/29/2009 8:24:37 AM ——————————————————— Welcome to Minitab, press F1 for help.

General Linear Model: HS DAS, Red versus F Umpan, IV Umpan, Suhu B MD Factor F Umpan IV Umpan Suhu B MD


Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for HS DAS, Red, using Adjusted SS for Tests Source P F Umpan 0.000 IV Umpan 0.000 Suhu B MD 0.000 F Umpan*IV Umpan 0.387 F Umpan*Suhu B MD 0.964 IV Umpan*Suhu B MD 0.868 F Umpan*IV Umpan*Suhu B MD 0.964 Error Total

S = 0.0440959

DF

Seq SS

Adj SS

Adj MS

F

2

0.107222

0.107222

0.053611

27.57

1

0.046944

0.046944

0.046944

24.14

2

0.060556

0.060556

0.030278

15.57

2

0.003889

0.003889

0.001944

1.00

4

0.001111

0.001111

0.000278

0.14

2

0.000556

0.000556

0.000278

0.14

4

0.001111

0.001111

0.000278

0.14

18 35

0.035000 0.256389

0.035000

0.001944

R-Sq = 86.35%

R-Sq(adj) = 73.46%


LAMPIRAN – 5B Results for: Worksheet 16 One-way ANOVA: HS DAS, Red_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total S = 0.05774

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.07000 0.05000 0.12000

MS 0.03500 0.00333

R-Sq = 58.33%

Mean 0.35000 0.45000 0.50000

StDev 0.05477 0.05477 0.06325

F 10.50

P 0.001

R-Sq(adj) = 52.78%

Individual 95% CIs For Mean Based on Pooled StDev -------+---------+---------+---------+-(------*------) (------*------) (------*-------) -------+---------+---------+---------+-0.350 0.420 0.490 0.560




Lower 0.02895 0.07895

F Umpan_0.6 5.75 6.00

--+---------+---------+---------+------(------*------) (------*------) --+---------+---------+---------+-------0.10 0.00 0.10 0.20

Center 0.10000 0.15000

Upper 0.17105 0.22105


Lower -0.02105

Center 0.05000

Upper 0.12105


F Umpan_0.6 6.00

--+---------+---------+---------+------(------*------) --+---------+---------+---------+-------0.10 0.00 0.10 0.20

LAMPIRAN – 5C One-way ANOVA: HS DAS, Red_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total S = 0.05676

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.04111 0.04833 0.08944

MS 0.02056 0.00322

R-Sq = 45.96%

Mean 0.45000 0.50000 0.56667

StDev 0.05477 0.06325 0.05164

F 6.38

P 0.010

R-Sq(adj) = 38.76%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(-------*-------) (-------*--------) (-------*--------) ---+---------+---------+---------+-----0.420 0.480 0.540 0.600




Lower -0.01985 0.04681

Center 0.05000 0.11667

Upper 0.11985 0.18652

F Umpan_0.7 5.75 6.00

----+---------+---------+---------+----(------*------) (------*------) ----+---------+---------+---------+-----0.10 0.00 0.10 0.20

F Umpan_0.7 = 5.75 subtracted from: F Umpan_0.7

Lower

Center

Upper


6.00

-0.00319

0.06667

0.13652

F Umpan_0.7 6.00

----+---------+---------+---------+----(------*------) ----+---------+---------+---------+-----0.10 0.00 0.10 0.20

LAMPIRAN – 5D Results for: Worksheet 17 One-way ANOVA: HS DAS, Red_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total S = 0.05477

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.03000 0.03000 0.06000

R-Sq = 50.00%

Mean 0.35000 0.45000

StDev 0.05477 0.05477

MS 0.03000 0.00300

F 10.00

P 0.010

R-Sq(adj) = 45.00%

Individual 95% CIs For Mean Based on Pooled StDev +---------+---------+---------+--------(---------*---------) (---------*---------) +---------+---------+---------+--------0.300 0.350 0.400 0.450




Lower 0.02954

Center 0.10000

Upper 0.17046

IV Umpan_5.50 0.7

+---------+---------+---------+--------(---------*---------) +---------+---------+---------+---------0.070 0.000 0.070 0.140


LAMPIRAN – 5D One-way ANOVA: HS DAS, Red_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total S = 0.05916

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.00750 0.03500 0.04250

R-Sq = 17.65%

Mean 0.45000 0.50000

StDev 0.05477 0.06325

MS 0.00750 0.00350

F 2.14

P 0.174

R-Sq(adj) = 9.41%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(-------------*------------) (------------*------------) -+---------+---------+---------+-------0.400 0.440 0.480 0.520




Lower -0.02611

Center 0.05000

Upper 0.12611

IV Umpan_5.75 0.7

---+---------+---------+---------+-----(-----------*------------) ---+---------+---------+---------+------0.060 0.000 0.060 0.120


LAMPIRAN – 5E One-way ANOVA: HS DAS, Red_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total S = 0.05774

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.01333 0.03333 0.04667

R-Sq = 28.57%

Mean 0.50000 0.56667

StDev 0.06325 0.05164

MS 0.01333 0.00333

F 4.00

P 0.073

R-Sq(adj) = 21.43%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(----------*----------) (---------*----------) -+---------+---------+---------+-------0.450 0.500 0.550 0.600




Lower -0.00760

Center 0.06667

Upper 0.14094

IV Umpan_6.00 0.7

--+---------+---------+---------+------(-----------*-----------) --+---------+---------+---------+-------0.060 0.000 0.060 0.120


LAMPIRAN – 5F Results for: Worksheet 18 One-way ANOVA: HS DAS, Red_218 versus F Umpan_218 Source F Umpan_218 Error Total S = 0.05270

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.03167 0.02500 0.05667

MS 0.01583 0.00278

R-Sq = 55.88%

Mean 0.35000 0.42500 0.47500

StDev 0.05774 0.05000 0.05000

F 5.70

P 0.025

R-Sq(adj) = 46.08%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (--------*--------) (--------*-------) (--------*-------) ---------+---------+---------+---------+ 0.350 0.420 0.490 0.560




Lower -0.00931 0.04069

Center 0.07500 0.12500

Upper 0.15931 0.20931

F Umpan_218 5.75

---+---------+---------+---------+-----(--------*-------)


6.00

(-------*--------) ---+---------+---------+---------+------0.10 0.00 0.10 0.20


Lower -0.03431

F Umpan_218 6.00

---+---------+---------+---------+-----(-------*-------) ---+---------+---------+---------+------0.10 0.00 0.10 0.20

Center 0.05000

Upper 0.13431

LAMPIRAN – 5G One-way ANOVA: HS DAS, Red_220 versus F Umpan_220 Source F Umpan_220 Error Total S = 0.06455

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.04500 0.03750 0.08250

MS 0.02250 0.00417

R-Sq = 54.55%

Mean 0.40000 0.47500 0.55000

StDev 0.08165 0.05000 0.05774

F 5.40

P 0.029

R-Sq(adj) = 44.44%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (--------*--------) (--------*---------) (--------*--------) ---------+---------+---------+---------+ 0.400 0.480 0.560 0.640




Lower -0.02825 0.04675

Center 0.07500 0.15000

Upper 0.17825 0.25325

F Umpan_220 5.75 6.00

-----+---------+---------+---------+---(-------*--------) (--------*-------)


-----+---------+---------+---------+----0.12 0.00 0.12 0.24


Lower -0.02825

Center 0.07500

Upper 0.17825

F Umpan_220 6.00

-----+---------+---------+---------+---(-------*--------) -----+---------+---------+---------+----0.12 0.00 0.12 0.24

LAMPIRAN – 5H One-way ANOVA: HS DAS, Red_222 versus F Umpan_222 Source F Umpan_222 Error Total S = 0.05270

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.03167 0.02500 0.05667

MS 0.01583 0.00278

R-Sq = 55.88%

Mean 0.45000 0.52500 0.57500

StDev 0.05774 0.05000 0.05000

F 5.70

P 0.025

R-Sq(adj) = 46.08%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(-------*--------) (--------*--------) (-------*--------) ----+---------+---------+---------+----0.420 0.490 0.560 0.630




Lower -0.00931 0.04069

Center 0.07500 0.12500

Upper 0.15931 0.20931

F Umpan_222

---+---------+---------+---------+------


5.75 6.00

(--------*-------) (-------*--------) ---+---------+---------+---------+------0.10 0.00 0.10 0.20


Lower -0.03431

Center 0.05000

Upper 0.13431

F Umpan_222 6.00

---+---------+---------+---------+-----(-------*-------) ---+---------+---------+---------+------0.10 0.00 0.10 0.20

LAMPIRAN – 5I Results for: Worksheet 19 One-way ANOVA: HS DAS, Red_5.50 versus Suhu B MD_5.50 Source Suhu B MD_5.50 Error Total S = 0.06667

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 0.02000 0.04000 0.06000

R-Sq = 33.33%

Mean 0.35000 0.40000 0.45000

StDev 0.05774 0.08165 0.05774

MS 0.01000 0.00444

F 2.25

P 0.161

R-Sq(adj) = 18.52%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(----------*----------) (----------*----------) (---------*----------) -+---------+---------+---------+-------0.280 0.350 0.420 0.490



Suhu B MD_5.50 = 218 subtracted from: Suhu B


MD_5.50 +--220 222 -)

Lower

Center

Upper

------+---------+---------+---------

-0.05664 -0.00664

0.05000 0.10000

0.15664 0.20664

(----------*----------) (----------*--------------+---------+---------+---------

+---0.10

0.00

0.10

0.20

Suhu B MD_5.50 = 220 subtracted from: Suhu B MD_5.50 +--222

Lower

Center

Upper

------+---------+---------+---------

-0.05664

0.05000

0.15664

(----------*----------) ------+---------+---------+---------

+---0.10

0.00

0.10

0.20

LAMPIRAN – 5J One-way ANOVA: HS DAS, Red_5.75 versus Suhu B MD_5.75 Source Suhu B MD_5.75 Error Total S = 0.05

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 0.02000 0.02250 0.04250

R-Sq = 47.06%

Mean 0.42500 0.47500 0.52500

StDev 0.05000 0.05000 0.05000

MS 0.01000 0.00250

F 4.00

P 0.057

R-Sq(adj) = 35.29%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (---------*--------) (--------*---------) (---------*--------) ---------+---------+---------+---------+ 0.420 0.480 0.540 0.600




Suhu B MD_5.75 = 218 subtracted from: Suhu B MD_5.75 +--220 222 --)

Lower

Center

Upper

------+---------+---------+---------

-0.02998 0.02002

0.05000 0.10000

0.12998 0.17998

(---------*---------) (--------*------------+---------+---------+---------

+---0.080

0.000

0.080

0.160

Suhu B MD_5.75 = 220 subtracted from: Suhu B MD_5.75 +--222

Lower

Center

Upper

------+---------+---------+---------

-0.02998

0.05000

0.12998

(---------*---------) ------+---------+---------+---------

+---0.080

0.000

0.080

0.160

LAMPIRAN – 5K One-way ANOVA: HS DAS, Red_6.00 versus Suhu B MD_6.00 Source Suhu B MD_6.00 Error Total S = 0.05270

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 0.02167 0.02500 0.04667

R-Sq = 46.43%

Mean 0.47500 0.55000 0.57500

StDev 0.05000 0.05774 0.05000

MS 0.01083 0.00278

F 3.90

P 0.060

R-Sq(adj) = 34.52%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(---------*---------) (---------*---------) (---------*---------) -+---------+---------+---------+-------0.420 0.480 0.540 0.600




All Pairwise Comparisons among Levels of Suhu B MD_6.00 Simultaneous confidence level = 88.66%

Suhu B MD_6.00 = 218 subtracted from: Suhu B MD_6.00 ---220 222 -)

Lower

Center

Upper

----+---------+---------+---------+-

-0.00931 0.01569

0.07500 0.10000

0.15931 0.18431

(---------*----------) (---------*------------+---------+---------+---------+-

----0.080

0.000

0.080

0.160

Suhu B MD_6.00 = 220 subtracted from: Suhu B MD_6.00 ---222

Lower

Center

Upper

----+---------+---------+---------+-

-0.05931

0.02500

0.10931

(---------*----------) ----+---------+---------+---------+-

----0.080

0.000

0.080

0.160

LAMPIRAN – 5L Results for: Worksheet 20 One-way ANOVA: HS DAS, Red_0.6 versus Suhu B MD_0.6 Source Suhu B MD_0.6 Error Total S = 0.07746

Level 218 220 222

N 6 6 6

DF 2 15 17

SS 0.03000 0.09000 0.12000

R-Sq = 25.00%

Mean 0.38333 0.43333 0.48333

StDev 0.07528 0.08165 0.07528

MS 0.01500 0.00600

F 2.50

P 0.116

R-Sq(adj) = 15.00%

Individual 95% CIs For Mean Based on Pooled StDev -------+---------+---------+---------+-(----------*----------) (----------*----------) (-----------*----------)


-------+---------+---------+---------+-0.360 0.420 0.480 0.540 Pooled StDev = 0.07746


Suhu B MD_0.6 = 218 subtracted from: Suhu B MD_0.6 --220 222

Lower

Center

Upper

-----+---------+---------+---------+-

-0.04532 0.00468

0.05000 0.10000

0.14532 0.19532

(---------*---------) (---------*---------) -----+---------+---------+---------+-

---0.10

0.00

0.10

0.20

Suhu B MD_0.6 = 220 subtracted from: Suhu B MD_0.6 --222

Lower

Center

Upper

-----+---------+---------+---------+-

-0.04532

0.05000

0.14532

(---------*---------) -----+---------+---------+---------+-

---0.10

0.00

0.10

0.20

LAMPIRAN – 5M One-way ANOVA: HS DAS, Red_0.7 versus Suhu B MD_0.7 Source Suhu B MD_0.7 Error Total S = 0.06236

DF 2 15 17

SS 0.03111 0.05833 0.08944

R-Sq = 34.78%

MS 0.01556 0.00389

F 4.00

P 0.041

R-Sq(adj) = 26.09%

Individual 95% CIs For Mean Based on


Level 218 220 222

N 6 6 6

Mean 0.45000 0.51667 0.55000

StDev 0.05477 0.07528 0.05477

Pooled StDev ----+---------+---------+---------+----(--------*--------) (--------*--------) (--------*--------) ----+---------+---------+---------+----0.600 0.420 0.480 0.540




Lower

Center

Upper

----+---------+---------+---------+--

-0.01007 0.02326

0.06667 0.10000

0.14341 0.17674

(--------*---------) (--------*---------) ----+---------+---------+---------+--

---0.080

0.000

0.080

0.160


Lower

Center

Upper

----+---------+---------+---------+--

-0.04341

0.03333

0.11007

(--------*---------) ----+---------+---------+---------+--

---0.080

0.000

0.080

0.160

LAMPIRAN – 5O Results for: Worksheet 21 One-way ANOVA: HS DAS, Red_218 versus IV Umpan_218 Source IV Umpan_218

DF 1

SS 0.01333

MS 0.01333

F 3.08

P 0.110


Error Total

10 11

S = 0.06583

R-Sq = 23.53%

Level 0.6 0.7

N 6 6

Mean 0.38333 0.45000

0.04333 0.05667

StDev 0.07528 0.05477

0.00433

R-Sq(adj) = 15.88%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(-----------*-----------) (-----------*-----------) -----+---------+---------+---------+---0.500 0.350 0.400 0.450




Lower -0.01802

Center 0.06667

Upper 0.15135

IV Umpan_218 0.7

----+---------+---------+---------+----(-------------*-------------) ----+---------+---------+---------+-----0.060 0.000 0.060 0.120

LAMPIRAN – 5P One-way ANOVA: HS DAS, Red_220 versus IV Umpan_220 Source IV Umpan_220

DF 1

SS 0.02083

MS 0.02083

F 3.38

P 0.096


Error Total

10 11

S = 0.07853

R-Sq = 25.25%

Level 0.6 0.7

N 6 6

Mean 0.43333 0.51667

0.06167 0.08250

StDev 0.08165 0.07528

0.00617

R-Sq(adj) = 17.78%

Individual 95% CIs For Mean Based on Pooled StDev +---------+---------+---------+--------(-----------*-----------) (-----------*-----------) +---------+---------+---------+--------0.360 0.420 0.480 0.540




Lower -0.01769

Center 0.08333

Upper 0.18435

IV Umpan_220 0.7

---+---------+---------+---------+-----(-----------*------------) ---+---------+---------+---------+------0.080 0.000 0.080 0.160

LAMPIRAN – 5Q One-way ANOVA: HS DAS, Red_222 versus IV Umpan_222


Source IV Umpan_222 Error Total

DF 1 10 11

S = 0.06583

R-Sq = 23.53%

Level 0.6 0.7

N 6 6

Mean 0.48333 0.55000

SS 0.01333 0.04333 0.05667

StDev 0.07528 0.05477

MS 0.01333 0.00433

F 3.08

P 0.110

R-Sq(adj) = 15.88%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(-----------*-----------) (-----------*-----------) -----+---------+---------+---------+---0.450 0.500 0.550 0.600




Lower -0.01802

Center 0.06667

Upper 0.15135

IV Umpan_222 0.7

----+---------+---------+---------+----(-------------*-------------) ----+---------+---------+---------+-----0.060 0.000 0.060 0.120

————— 8/2/2009 8:41:36 AM ———————————————————

LAMPIRAN -6A


————— 5/8/2009 6:04:08 AM ——————————————————— General Linear Model: HS AS Yellow versus F Umpan, IV Umpan, Suhu B MD Factor F Umpan IV Umpan Suhu B MD


Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for HS AS Yellow, using Adjusted SS for Tests Source P F Umpan 0.034 IV Umpan 0.007 Suhu B MD 0.000 F Umpan*IV Umpan 0.837 F Umpan*Suhu B MD 0.942 IV Umpan*Suhu B MD 0.175 F Umpan*IV Umpan*Suhu B MD 0.946 Error Total

S = 0.180278

DF

Seq SS

Adj SS

Adj MS

F

2

0.26722

0.26722

0.13361

4.11

1

0.30250

0.30250

0.30250

9.31

2

15.58389

15.58389

7.79194

239.75

2

0.01167

0.01167

0.00583

0.18

4

0.02444

0.02444

0.00611

0.19

2

0.12500

0.12500

0.06250

1.92

4

0.02333

0.02333

0.00583

0.18

18 35

0.58500 16.92306

0.58500

0.03250

R-Sq = 96.54%

R-Sq(adj) = 93.28%


LAMPIRAN -6B ————— 5/8/2009 10:38:31 AM ——————————————————— One-way ANOVA: HS AS Yellow_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total

DF 2 15 17

S = 0.6813

R-Sq = 1.99%

Level 5.50 5.75 6.00

N 6 6 6

SS 0.141 6.963 7.104

Mean 4.6333 4.7500 4.8500

MS 0.071 0.464

StDev 0.7062 0.6834 0.6535

F 0.15

P 0.860

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (--------------*--------------) (--------------*--------------) (--------------*--------------) ---------+---------+---------+---------+ 4.40 4.80 5.20 5.60



F Umpan_0.6 = 5.50 subtracted from: F Umpan_0.6 --+ 5.75 -) 6.00 ---)

Lower

Center

Upper

---------+---------+---------+-------

-0.7218

0.1167

0.9551

(---------------*---------------

-0.6218

0.2167

1.0551

(---------------*---------------------+---------+---------+-------

--+ -0.50

0.00

0.50

1.00

F Umpan_0.6 = 5.75 subtracted from: F Umpan_0.6 --+ 6.00 -)

Lower

Center

Upper

---------+---------+---------+-------

-0.7385

0.1000

0.9385

(----------------*-----------------------+---------+---------+-------

--+ -0.50

0.00

0.50

1.00


LAMPIRAN -6C ————— 5/8/2009 10:38:31 AM ——————————————————— One-way ANOVA: HS DAS Yellow_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total

DF 2 15 17

S = 0.7907

R-Sq = 1.45%

Level 5.50 5.75 6.00

N 6 6 6

Mean 4.8500 4.8833 5.0500

SS 0.138 9.378 9.516

MS 0.069 0.625

StDev 0.7740 0.7782 0.8191

F 0.11

P 0.896

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(----------------*----------------) (----------------*----------------) (----------------*----------------) ------+---------+---------+---------+--4.40 4.80 5.20 5.60



F Umpan_0.7 = 5.50 subtracted from: F Umpan_0.7 --+ 5.75 6.00 --)

Lower

Center

Upper

---------+---------+---------+-------

-0.9397 -0.7730

0.0333 0.2000

1.0064 1.1730

(----------------*---------------) (---------------*----------------------+---------+---------+-------

--+ -0.60

0.00

0.60

1.20

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7 --+ 6.00 -)

Lower

Center

Upper

---------+---------+---------+-------

-0.8064

0.1667

1.1397

(---------------*----------------------+---------+---------+-------

--+ -0.60

0.00

0.60

1.20

LAMPIRAN -6D ————— 5/27/2009 10:40:11 AM —————————————————— One-way ANOVA: HS AS Yellow_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total S = 0.7408

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.141 5.488 5.629

R-Sq = 2.50%

Mean 4.6333 4.8500

StDev 0.7062 0.7740

MS 0.141 0.549

F 0.26

P 0.623

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(----------------*----------------) (----------------*----------------) -+---------+---------+---------+-------4.00 4.40 4.80 5.20




Lower -0.7364

IV Umpan_5.50 0.7

------+---------+---------+---------+--(---------------*--------------)

Center 0.2167

Upper 1.1697


------+---------+---------+---------+---0.60 0.00 0.60 1.20 MTB > Oneway 'HS AS Yellow_5.75' 'IV Umpan_5.75'; SUBC> Fisher 5.

LAMPIRAN -6E ————— 5/27/2009 10:40:11 AM —————————————————— One-way ANOVA: HS AS Yellow_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total S = 0.7323

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.053 5.363 5.417

R-Sq = 0.98%

Mean 4.7500 4.8833

StDev 0.6834 0.7782

MS 0.053 0.536

F 0.10

P 0.759

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(----------------*---------------) (----------------*----------------) --------+---------+---------+---------+4.40 4.80 5.20 5.60




Lower -0.8088

Center 0.1333

Upper 1.0754

IV Umpan_5.75

------+---------+---------+---------+---


0.7

(--------------*---------------) ------+---------+---------+---------+---0.60 0.00 0.60 1.20

LAMPIRAN -6F ————— 5/27/2009 10:40:11 AM —————————————————— One-way ANOVA: HS AS Yellow_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total S = 0.7409

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.120 5.490 5.610

R-Sq = 2.14%

Mean 4.8500 5.0500

StDev 0.6535 0.8191

MS 0.120 0.549

F 0.22

P 0.650

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(----------------*----------------) (----------------*----------------) ------+---------+---------+---------+--4.40 4.80 5.20 5.60




Lower -0.7532

Center 0.2000

Upper 1.1532


IV Umpan_6.00 0.7

------+---------+---------+---------+--(---------------*---------------) ------+---------+---------+---------+---0.60 0.00 0.60 1.20

LAMPIRAN -6G ————— 5/27/2009 10:40:11 AM —————————————————— One-way ANOVA: HS AS Yellow_218 versus F Umpan_218 Source F Umpan_218 Error Total

DF 2 9 11

S = 0.1269

R-Sq = 42.00%

Level 5.50 5.75 6.00

N 4 4 4

Mean 3.8500 3.9250 4.0750

SS 0.1050 0.1450 0.2500

StDev 0.1732 0.0957 0.0957

MS 0.0525 0.0161

F 3.26

P 0.086

R-Sq(adj) = 29.11%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(---------*--------) (---------*--------) (---------*--------) ---+---------+---------+---------+-----3.75 3.90 4.05 4.20



F Umpan_218 = 5.50 subtracted from:


F Umpan_218 ---+5.75 6.00 ----)

Lower

Center

Upper

--------+---------+---------+------

-0.1280 0.0220

0.0750 0.2250

0.2780 0.4280

(---------*---------) (---------*------------+---------+---------+------

---+-0.20

0.00

0.20

0.40

F Umpan_218 = 5.75 subtracted from: F Umpan_218 ---+6.00 -)

Lower

Center

Upper

--------+---------+---------+------

-0.0530

0.1500

0.3530

(---------*----------------+---------+---------+------

---+-0.20

0.00

0.20

0.40

LAMPIRAN -6H ————— 5/27/2009 10:40:11 AM —————————————————— MTB > Oneway 'HS AS Yellow_220' 'F Umpan_220'; SUBC> Fisher 5.

One-way ANOVA: HS AS Yellow_220 versus F Umpan_220 Source F Umpan_220 Error Total

DF 2 9 11

S = 0.1886

R-Sq = 12.73%

Level 5.50 5.75 6.00

N 4 4 4

Mean 4.9500 5.0500 5.1000

SS 0.0467 0.3200 0.3667

StDev 0.1915 0.1915 0.1826

MS 0.0233 0.0356

F 0.66

P 0.542

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(-------------*-------------) (--------------*-------------) (-------------*-------------) ----+---------+---------+---------+----4.80 4.95 5.10 5.25




All Pairwise Comparisons among Levels of F Umpan_220 Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from: F Umpan_220 +----5.75 6.00

Lower

Center

Upper

----+---------+---------+---------

-0.2016 -0.1516

0.1000 0.1500

0.4016 0.4516

(-----------*-----------) (-----------*-----------) ----+---------+---------+---------

+-----0.25

0.00

0.25

0.50

F Umpan_220 = 5.75 subtracted from: F Umpan_220 +----6.00

Lower

Center

Upper

----+---------+---------+---------

-0.2516

0.0500

0.3516

(-----------*-----------) ----+---------+---------+---------

+-----0.25

0.00

0.25

0.50

LAMPIRAN -6I ————— 5/27/2009 10:40:11 AM —————————————————— MTB > Oneway 'HS AS Yellow_222' 'F Umpan_222'; SUBC> Fisher 5.

One-way ANOVA: HS AS Yellow_222 versus F Umpan_222 Source F Umpan_222 Error Total

DF 2 9 11

S = 0.2544

R-Sq = 19.38%

Level 5.50 5.75 6.00

N 4 4 4

Mean 5.4250 5.4750 5.6750

SS 0.1400 0.5825 0.7225

StDev 0.2630 0.2217 0.2754

MS 0.0700 0.0647

F 1.08

P 0.379

R-Sq(adj) = 1.46%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(-----------*-----------) (-----------*-----------) (-----------*-----------) -----+---------+---------+---------+---5.25 5.50 5.75 6.00




F Umpan_222 = 5.50 subtracted from: F Umpan_222 --+-5.75 6.00 -)

Lower

Center

Upper

-------+---------+---------+-------

-0.3569 -0.1569

0.0500 0.2500

0.4569 0.6569

(----------*-----------) (----------*----------------+---------+---------+-------

--+--0.35

0.00

0.35

0.70

F Umpan_222 = 5.75 subtracted from: F Umpan_222 --+-6.00

Lower

Center

Upper

-------+---------+---------+-------

-0.2069

0.2000

0.6069

(-----------*----------) -------+---------+---------+-------

--+--0.35

0.00

0.35

0.70

LAMPIRAN -6J MTB > Oneway 'HS AS Yellow_5.50' 'Suhu B MD_5.50'; SUBC> Fisher 5.

One-way ANOVA: HS AS Yellow_5.50 versus Suhu B MD_5.50 Source Suhu B MD_5.50 Error Total S = 0.2128

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 5.2217 0.4075 5.6292

R-Sq = 92.76%

Mean 3.8500 4.9500 5.4250

StDev 0.1732 0.1915 0.2630

MS 2.6108 0.0453

F 57.66

P 0.000

R-Sq(adj) = 91.15%

Individual 95% CIs For Mean Based on Pooled StDev +---------+---------+---------+--------(---*---) (----*---) (---*---) +---------+---------+---------+--------3.60 4.20 4.80 5.40




Suhu B MD_5.50 = 218 subtracted from: Suhu B MD_5.50 220 222 )

Lower

Center

Upper

--+---------+---------+---------+------

0.7596 1.2346

1.1000 1.5750

1.4404 1.9154

(----*----) (---*-----+---------+---------+---------+------

-0.70

0.00

0.70

1.40


Lower

Center

Upper

--+---------+---------+---------+------

0.1346

0.4750

0.8154

(----*----) --+---------+---------+---------+------

-0.70

0.00

0.70

1.40

LAMPIRAN -6K MTB > Oneway 'HS AS Yellow_5.75' 'Suhu B MD_5.75'; SUBC> Fisher 5.


Level

N

DF 2 9 11

SS 5.1317 0.2850 5.4167

R-Sq = 94.74%

Mean

StDev

MS 2.5658 0.0317

F 81.03

P 0.000

R-Sq(adj) = 93.57%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+---


218 220 222

4 4 4

3.9250 5.0500 5.4750

0.0957 0.1915 0.2217

(----*---) (---*---) (---*----) ------+---------+---------+---------+--5.50 4.00 4.50 5.00




Lower

Center

Upper

+---------+---------+---------+------

0.8404 1.2654

1.1250 1.5500

1.4096 1.8346

(---*---) (---*---) +---------+---------+---------+------

---0.70

0.00

0.70

1.40


Lower

Center

Upper

+---------+---------+---------+------

0.1404

0.4250

0.7096

(---*---) +---------+---------+---------+------

---0.70

0.00

0.70

1.40

LAMPIRAN -6L MTB > Oneway 'HS AS Yellow_6.00' 'Suhu B MD_6.00'; SUBC> Fisher 5.


DF 2 9 11

SS 5.2550 0.3550 5.6100

R-Sq = 93.67%

MS 2.6275 0.0394

F 66.61

P 0.000

R-Sq(adj) = 92.27%


Level 218 220 222

N 4 4 4

Mean 4.0750 5.1000 5.6750

StDev 0.0957 0.1826 0.2754

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(---*---) (---*---) (---*--) ------+---------+---------+---------+--5.40 6.00 4.20 4.80



Suhu B MD_6.00 = 218 subtracted from: Suhu B MD_6.00 -220 222

Lower

Center

Upper

-+---------+---------+---------+------

0.7073 1.2823

1.0250 1.6000

1.3427 1.9177

(---*---) (---*---) -+---------+---------+---------+------

--0.80

0.00

0.80

1.60

Suhu B MD_6.00 = 220 subtracted from: Suhu B MD_6.00 -222

Lower

Center

Upper

-+---------+---------+---------+------

0.2573

0.5750

0.8927

(---*---) -+---------+---------+---------+------

--0.80

0.00

0.80

1.60

LAMPIRAN -6M ————— 5/8/2009 6:04:08 AM ——————————————————— MTB > Oneway 'HS AS Yellow_0.6' 'Suhu B MD_0.6'; SUBC> Fisher 5.



Level 218 220 222

N 6 6 6

DF 2 15 17

SS 6.8211 0.2833 7.1044

MS 3.4106 0.0189

R-Sq = 96.01%

Mean 3.9000 4.9833 5.3500

StDev 0.1549 0.1472 0.1049

F 180.56

P 0.000

R-Sq(adj) = 95.48%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(-*-) (--*-) (-*-) ----+---------+---------+---------+----4.00 4.50 5.00 5.50




Lower 0.9142 1.2809

Center 1.0833 1.4500

Upper 1.2525 1.6191

---------+---------+---------+---------+ (--*--) (--*--) ---------+---------+---------+---------+ 0.00 0.60 1.20 1.80


Lower 0.1975

Center 0.3667

Upper 0.5358

---------+---------+---------+---------+ (--*--) ---------+---------+---------+---------+ 0.00 0.60 1.20 1.80

LAMPIRAN -6N ————— 5/8/2009 6:04:08 AM ——————————————————— MTB > Oneway 'HS AS Yellow_0.7' 'Suhu B MD_0.7';


SUBC>

Fisher 5.


Level 218 220 222

N 6 6 6

DF 2 15 17

SS 8.8878 0.6283 9.5161

MS 4.4439 0.0419

R-Sq = 93.40%

Mean 4.0000 5.0833 5.7000

StDev 0.1414 0.2137 0.2449

F 106.09

P 0.000

R-Sq(adj) = 92.52%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--*--) (--*--) (--*--) ------+---------+---------+---------+--4.20 4.80 5.40 6.00




Lower

Center

Upper

-+---------+---------+---------+-------

0.8315 1.4481

1.0833 1.7000

1.3352 1.9519

(---*--) (--*--) -+---------+---------+---------+-------

-0.80

0.00

0.80

1.60


Lower

Center

Upper

-+---------+---------+---------+-------

0.3648

0.6167

0.8685

(--*--) -+---------+---------+---------+-------

-0.80

0.00

0.80

1.60


LAMPIRAN -6O ————— 7/10/2009 7:46:39 AM ———————————————————

Welcome to Minitab, press F1 for help. Retrieving project from file: 'C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23' MTB > Unstack ( 'IV Umpan' 'HS AS Yellow'); SUBC> Subscripts 'Suhu B MD'; SUBC> NewWS; SUBC> VarNames.

Results for: Worksheet 8 MTB > Oneway 'HS AS Yellow_218' 'IV Umpan_218'; SUBC> Fisher 5.

One-way ANOVA: HS AS Yellow_218 versus IV Umpan_218 Source IV Umpan_218 Error Total S = 0.1483

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.0300 0.2200 0.2500

MS 0.0300 0.0220

R-Sq = 12.00%

Mean 3.9000 4.0000

StDev 0.1549 0.1414

F 1.36

P 0.270

R-Sq(adj) = 3.20%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(------------*------------) (------------*------------) ---+---------+---------+---------+-----3.80 3.90 4.00 4.10



IV Umpan_218 = 0.6 subtracted from: IV Umpan_218 +-----0.7

Lower

Center

Upper

---+---------+---------+---------

-0.0908

0.1000

0.2908

(------------*-----------) ---+---------+---------+---------

+------0.15

0.00

0.15

0.30


LAMPIRAN -6P MTB > Oneway 'HS AS Yellow_220' 'IV Umpan_220'; SUBC> Fisher 5.


Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.0300 0.3367 0.3667

R-Sq = 8.18%

Mean 4.9833 5.0833

StDev 0.1472 0.2137

MS 0.0300 0.0337

F 0.89

P 0.367

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (-------------*-------------) (-------------*-------------) ---------+---------+---------+---------+ 4.92 5.04 5.16 5.28



IV Umpan_220 = 0.6 subtracted from: IV Umpan_220 --+--0.7 ----)

Lower

Center

Upper

------+---------+---------+-------

-0.1360

0.1000

0.3360

(---------------*---------------+---------+---------+-------

--+---0.15

0.00

0.15

0.30


LAMPIRAN -6Q MTB > Oneway 'HS AS Yellow_222' 'IV Umpan_222'; SUBC> Fisher 5.


Level 0.6 0.7

N 6 6

DF 1 10 11

SS 0.3675 0.3550 0.7225

MS 0.3675 0.0355

R-Sq = 50.87%

Mean 5.3500 5.7000

StDev 0.1049 0.2449

F 10.35

P 0.009

R-Sq(adj) = 45.95%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(--------*-------) (--------*--------) -+---------+---------+---------+-------5.20 5.40 5.60 5.80




Lower 0.1076

Center 0.3500

Upper 0.5924

IV Umpan_222 0.7

+---------+---------+---------+--------(---------*---------) +---------+---------+---------+---------0.25 0.00 0.25 0.50

MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23"; SUBC> Project; SUBC> Replace. Saving file as: 'C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23' Existing file replaced. MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23"; SUBC> Project; SUBC> Replace.

————— 7/10/2009 8:31:46 PM ——————————————————


LAMPIRAN – 7A ————— 8/17/2009 6:22:32 PM ——————————————————— Welcome to Minitab, press F1 for help.

General Linear Model: AV Residue versus F Umpan, IV Umpan, Suhu BMD Factor F Umpan IV Umpan Suhu BMD


Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for AV Residue, using Adjusted SS for Tests Source F Umpan IV Umpan Suhu BMD F Umpan*IV Umpan F Umpan*Suhu BMD IV Umpan*Suhu BMD F Umpan*IV Umpan*Suhu BMD Error Total

S = 1.21906

DF 2 1 2 2 4 2 4 18 35

R-Sq = 94.69%

Seq SS 0.344 135.334 294.976 0.341 0.101 45.802 0.288 26.750 503.936

Adj SS 0.344 135.334 294.976 0.341 0.101 45.802 0.288 26.750

Adj MS 0.172 135.334 147.488 0.170 0.025 22.901 0.072 1.486

F 0.12 91.07 99.24 0.11 0.02 15.41 0.05

P 0.891 0.000 0.000 0.892 0.999 0.000 0.995

R-Sq(adj) = 89.68%


LAMPIRAN – 7B Results for: Worksheet 3 One-way ANOVA: AV Residue_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total S = 1.948

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.13 56.94 57.07

MS 0.06 3.80

R-Sq = 0.23%

Mean 25.533 25.733 25.683

StDev 2.023 1.908 1.913

F 0.02

P 0.983

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(----------------*----------------) (----------------*----------------) (----------------*----------------) --+---------+---------+---------+------24.0 25.0 26.0 27.0



F Umpan_0.6 = 5.50 subtracted from: F Umpan_0.6 +--5.75 6.00

Lower

Center

Upper

------+---------+---------+---------

-2.197 -2.247

0.200 0.150

2.597 2.547

(---------------*---------------) (---------------*---------------) ------+---------+---------+---------

+---1.5

0.0

1.5

3.0

F Umpan_0.6 = 5.75 subtracted from: F Umpan_0.6 +--6.00

Lower

Center

Upper

------+---------+---------+---------

-2.447

-0.050

2.347

(---------------*---------------) ------+---------+---------+---------

+---1.5

0.0

1.5

3.0


LAMPIRAN – 7C One-way ANOVA: AV Residue_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total S = 4.553

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 0.6 311.0 311.5

R-Sq = 0.18%

Mean 29.467 29.350 29.767

StDev 4.493 4.569 4.597

MS 0.3 20.7

F 0.01

P 0.987

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(---------------*---------------) (--------------*---------------) (---------------*---------------) --------+---------+---------+---------+27.5 30.0 32.5 35.0



F Umpan_0.7 = 5.50 subtracted from: F Umpan_0.7 +-5.75 6.00

Lower

Center

Upper

-------+---------+---------+---------

-5.720 -5.303

-0.117 0.300

5.487 5.903

(---------------*---------------) (---------------*---------------) -------+---------+---------+---------

+--3.5

0.0

3.5

7.0

F Umpan_0.7 = 5.75 subtracted from: F Umpan_0.7 +--

Lower

Center

Upper

-------+---------+---------+---------


6.00

-5.187

0.417

6.020

(---------------*---------------) -------+---------+---------+---------

+--3.5

0.0

3.5

7.0

LAMPIRAN – 7D Results for: Worksheet 4 One-way ANOVA: AV Residue_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total S = 3.484

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 46.4 121.4 167.8

MS 46.4 12.1

R-Sq = 27.66%

Mean 25.533 29.467

StDev 2.023 4.493

F 3.82

P 0.079

R-Sq(adj) = 20.43%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(---------*----------) (---------*----------) -----+---------+---------+---------+---24.0 27.0 30.0 33.0



IV Umpan_5.50 = 0.6 subtracted from: IV Umpan_5.50 ----0.7 --)

Lower

Center

Upper

---+---------+---------+---------+-

-0.549

3.933

8.415

(------------*----------


---+---------+---------+---------+-----3.5

0.0

3.5

7.0

LAMPIRAN – 7E One-way ANOVA: AV Residue_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total S = 3.501

DF 1 10 11

SS 39.2 122.6 161.8

MS 39.2 12.3

R-Sq = 24.25%

F 3.20

P 0.104

R-Sq(adj) = 16.67%

Individual 95% CIs For Mean Based on Pooled StDev Level 0.6 0.7

N 6 6

Mean 25.733 29.350

StDev 1.908 4.569

+---------+---------+---------+--------(------------*------------) (-----------*------------) +---------+---------+---------+--------22.5 25.0 27.5 30.0



IV Umpan_5.75 = 0.6 subtracted from: IV Umpan_5.75 ----0.7 -)

Lower

Center

Upper

---+---------+---------+---------+-

-0.887

3.617

8.121

(------------*-----------


---+---------+---------+---------+-----3.5

0.0

3.5

7.0

LAMPIRAN – 7F One-way ANOVA: AV Residue_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total S = 3.521

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 50.0 123.9 174.0

MS 50.0 12.4

R-Sq = 28.75%

Mean 25.683 29.767

StDev 1.913 4.597

F 4.04

P 0.072

R-Sq(adj) = 21.63%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(----------*---------) (---------*----------) -----+---------+---------+---------+---24.0 27.0 30.0 33.0



IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00 ----0.7 ---)

Lower

Center

Upper

---+---------+---------+---------+-

-0.446

4.083

8.612

(------------*-----------+---------+---------+---------+-

-----3.5

0.0

3.5

7.0

LAMPIRAN – 7G Results for: Worksheet 5 One-way ANOVA: AV Residue_218 versus F Umpan_218 Source F Umpan_218 Error Total S = 4.260

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.2 163.3 163.5

R-Sq = 0.11%

MS 0.1 18.1

Mean 31.525 31.575 31.800

StDev 4.200 4.127 4.445

F 0.00

P 0.995

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(------------------*------------------) (------------------*-------------------) (------------------*------------------) ---+---------+---------+---------+-----27.5 30.0 32.5 35.0


Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of F Umpan_218



F Umpan_218 = 5.50 subtracted from: F Umpan_218 -+5.75 6.00

Lower

Center

Upper

--------+---------+---------+--------

-6.764 -6.539

0.050 0.275

6.864 7.089

(----------------*----------------) (----------------*----------------) --------+---------+---------+--------

-+-4.0

0.0

4.0

8.0

F Umpan_218 = 5.75 subtracted from: F Umpan_218 -+6.00

Lower

Center

Upper

--------+---------+---------+--------

-6.589

0.225

7.039

(----------------*----------------) --------+---------+---------+--------

-+-4.0

0.0

4.0

8.0

LAMPIRAN – 7H One-way ANOVA: AV Residue_220 versus F Umpan_220 Source F Umpan_220 Error Total S = 1.547

Level 5.50 5.75 6.00

N 4 4 4

DF 2 9 11

SS 0.21 21.53 21.74

MS 0.11 2.39

R-Sq = 0.97%

Mean 25.550 25.725 25.875

StDev 1.816 1.408 1.377

F 0.04

P 0.957

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(----------------*-----------------) (----------------*-----------------) (-----------------*----------------) --+---------+---------+---------+------24.0 25.0 26.0 27.0




F Umpan_220 = 5.50 subtracted from: F Umpan_220 +-5.75 6.00

Lower

Center

Upper

-------+---------+---------+---------

-2.299 -2.149

0.175 0.325

2.649 2.799

(---------------*----------------) (---------------*----------------) -------+---------+---------+---------

+--1.5

0.0

1.5

3.0

F Umpan_220 = 5.75 subtracted from: F Umpan_220 +-6.00

Lower

Center

Upper

-------+---------+---------+---------

-2.324

0.150

2.624

(---------------*---------------) -------+---------+---------+---------

+--1.5

0.0

1.5

3.0

LAMPIRAN – 7I One-way ANOVA: AV Residue_222 versus F Umpan_222 Source F Umpan_222 Error Total S = 1.623

DF 2 9 11

SS 0.06 23.69 23.76

MS 0.03 2.63

R-Sq = 0.26%

F 0.01

P 0.988

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Level 5.50 5.75 6.00

N 4 4 4

Mean 25.425 25.325 25.500

StDev 1.607 1.513 1.740

Pooled StDev -----+---------+---------+---------+---(-----------------*------------------) (-----------------*------------------) (-----------------*-----------------) -----+---------+---------+---------+---24.0 25.0 26.0 27.0



F Umpan_222 = 5.50 subtracted from: F Umpan_222 -+5.75 6.00

Lower

Center

Upper

--------+---------+---------+--------

-2.695 -2.520

-0.100 0.075

2.495 2.670

(----------------*-----------------) (----------------*-----------------) --------+---------+---------+--------

-+-1.5

0.0

1.5

3.0

F Umpan_222 = 5.75 subtracted from: F Umpan_222 -+6.00

Lower

Center

Upper

--------+---------+---------+--------

-2.420

0.175

2.770

(----------------*----------------) --------+---------+---------+--------

-+-1.5

0.0

1.5

3.0

LAMPIRAN – 7J Results for: Worksheet 4 One-way ANOVA: AV Residue_5.50 versus Suhu BMD_5.50


Source Suhu BMD_5.50 Error Total S = 2.800

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 97.24 70.56 167.80

R-Sq = 57.95%

Mean 31.525 25.550 25.425

StDev 4.200 1.816 1.607

MS 48.62 7.84

F 6.20

P 0.020

R-Sq(adj) = 48.60%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--------*--------) (--------*--------) (--------*--------) ------+---------+---------+---------+--24.5 28.0 31.5 35.0


Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of Suhu BMD_5.50 Simultaneous confidence level = 88.66%

Suhu BMD_5.50 = 218 subtracted from: Suhu BMD_5.50 -220 222

Lower

Center

Upper

------+---------+---------+---------+-

-10.454 -10.579

-5.975 -6.100

-1.496 -1.621

(----------*----------) (----------*----------) ------+---------+---------+---------+-

--8.0

-4.0

0.0

4.0

Suhu BMD_5.50 = 220 subtracted from: Suhu BMD_5.50 222

Lower -4.604

Center -0.125

Upper 4.354

------+---------+---------+---------+--(-----------*----------) ------+---------+---------+---------+---8.0 -4.0 0.0 4.0

LAMPIRAN – 7K


One-way ANOVA: AV Residue_5.75 versus Suhu BMD_5.75 Source Suhu BMD_5.75 Error Total S = 2.665

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 97.93 63.90 161.83

R-Sq = 60.51%

Mean 31.575 25.725 25.325

StDev 4.127 1.408 1.513

MS 48.96 7.10

F 6.90

P 0.015

R-Sq(adj) = 51.74%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(-------*--------) (--------*-------) (-------*--------) ------+---------+---------+---------+--24.5 28.0 31.5 35.0



Suhu BMD_5.75 = 218 subtracted from: Suhu BMD_5.75 -220 222

Lower

Center

Upper

------+---------+---------+---------+-

-10.112 -10.512

-5.850 -6.250

-1.588 -1.988

(---------*----------) (---------*----------) ------+---------+---------+---------+-

--8.0

-4.0

0.0

4.0


Lower -4.662

Center -0.400

Upper 3.862

------+---------+---------+---------+--(----------*----------) ------+---------+---------+---------+---8.0 -4.0 0.0 4.0


LAMPIRAN – 7L One-way ANOVA: AV Residue_6.00 versus Suhu BMD_6.00 Source Suhu BMD_6.00 Error Total S = 2.868

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 99.91 74.05 173.96

R-Sq = 57.43%

Mean 31.800 25.875 25.500

StDev 4.445 1.377 1.740

MS 49.96 8.23

F 6.07

P 0.021

R-Sq(adj) = 47.98%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--------*--------) (--------*--------) (--------*--------) ------+---------+---------+---------+--24.5 28.0 31.5 35.0



Suhu BMD_6.00 = 218 subtracted from: Suhu BMD_6.00 +-220 222

Lower

Center

Upper

-------+---------+---------+---------

-10.513 -10.888

-5.925 -6.300

-1.337 -1.712

(----------*-----------) (----------*-----------) -------+---------+---------+---------

+--8.0

-4.0

0.0

4.0


Lower -4.963

Center -0.375

Upper 4.213

-------+---------+---------+---------+-(----------*-----------) -------+---------+---------+---------+--8.0 -4.0 0.0 4.0


LAMPIRAN – 7M Results for: Worksheet 3 One-way ANOVA: AV Residue_0.6 versus Suhu BMD_0.6 Source Suhu BMD_0.6 Error Total S = 0.4398

Level 218 220 222

N 6 6 6

DF 2 15 17

SS 54.163 2.902 57.065

MS 27.082 0.193

R-Sq = 94.92%

Mean 28.100 24.533 24.317

StDev 0.283 0.372 0.601

F 140.00

P 0.000

R-Sq(adj) = 94.24%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(--*--) (--*---) (---*--) -+---------+---------+---------+-------24.0 25.2 26.4 27.6



Suhu BMD_0.6 = 218 subtracted from: Suhu BMD_0.6 --+ 220 222

Lower

Center

Upper

---------+---------+---------+-------

-4.1079 -4.3246

-3.5667 -3.7833

-3.0254 -3.2421

(--*---) (---*--) ---------+---------+---------+-------

--+ -3.0

-1.5

0.0

1.5

Suhu BMD_0.6 = 220 subtracted from: Suhu BMD_0.6 -+ 222

Lower

Center

Upper

---------+---------+---------+--------

-0.7579

-0.2167

0.3246

(---*--) ---------+---------+---------+--------

-+ -3.0

-1.5

0.0

1.5


LAMPIRAN – 7N One-way ANOVA: AV Residue_0.7 versus Suhu BMD_0.7 Source Suhu BMD_0.7 Error Total S = 1.289

Level 218 220 222

N 6 6 6

DF 2 15 17

SS 286.61 24.92 311.54

MS 143.31 1.66

R-Sq = 92.00%

Mean 35.167 26.900 26.517

StDev 1.628 0.921 1.219

F 86.25

P 0.000

R-Sq(adj) = 90.93%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(---*---) (---*--) (--*---) -----+---------+---------+---------+---27.0 30.0 33.0 36.0



Suhu BMD_0.7 = 218 subtracted from: Suhu BMD_0.7 + 220 222

Lower

Center

Upper

---------+---------+---------+---------

-9.853 -10.236

-8.267 -8.650

-6.680 -7.064

(---*----) (---*----) ---------+---------+---------+---------

+ -7.0

-3.5

0.0

3.5


Lower -1.970

Center -0.383

Upper 1.203

---------+---------+---------+---------+ (----*---) ---------+---------+---------+---------+ -7.0 -3.5 0.0 3.5


LAMPIRAN – 7O Results for: Worksheet 5 One-way ANOVA: AV Residue_218 versus IV Umpan_218 Source IV Umpan_218 Error Total S = 1.168

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 149.81 13.65 163.47

MS 149.81 1.37

R-Sq = 91.65%

Mean 28.100 35.167

StDev 0.283 1.628

F 109.73

P 0.000

R-Sq(adj) = 90.81%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(---*----) (----*---) --+---------+---------+---------+------27.5 30.0 32.5 35.0



IV Umpan_218 = 0.6 subtracted from: IV Umpan_218 --0.7

Lower

Center

Upper

-----+---------+---------+---------+-

5.564

7.067

8.570

(----*----) -----+---------+---------+---------+-

--0.0

3.0

6.0

9.0


LAMPIRAN – 7P One-way ANOVA: AV Residue_220 versus IV Umpan_220 Source IV Umpan_220 Error Total S = 0.7024

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 16.803 4.933 21.737

MS 16.803 0.493

R-Sq = 77.30%

Mean 24.533 26.900

StDev 0.372 0.921

F 34.06

P 0.000

R-Sq(adj) = 75.03%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(-----*------) (-----*-----) -+---------+---------+---------+-------24.0 25.0 26.0 27.0



IV Umpan_220 = 0.6 subtracted from: IV Umpan_220 ---+0.7 )

Lower

Center

Upper

--------+---------+---------+------

1.4631

2.3667

3.2702

(-------*-------------+---------+---------+------

---+0.0

1.2

2.4

3.6


LAMPIRAN – 7Q One-way ANOVA: AV Residue_222 versus IV Umpan_222 Source IV Umpan_222 Error Total S = 0.9611

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 14.520 9.237 23.757

MS 14.520 0.924

R-Sq = 61.12%

Mean 24.317 26.517

StDev 0.601 1.219

F 15.72

P 0.003

R-Sq(adj) = 57.23%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+--(--------*--------) (--------*--------) ------+---------+---------+---------+--24.0 25.0 26.0 27.0




Lower 0.9637

Center 2.2000

Upper 3.4363

IV Umpan_222 0.7

+---------+---------+---------+--------(---------*----------) +---------+---------+---------+---------1.2 0.0 1.2 2.4


LAMPIRAN – 8A ————— 12/18/2009 11:03:21 PM —————————————————— Welcome to Minitab, press F1 for help.

General Linear Model: Res Yield versus F Umpan, IV Umpan, Suhu MD Factor F Umpan IV Umpan Suhu MD


Levels 3 2 3

Values 5.50, 5.75, 6.00 0.6, 0.7 218, 220, 222

Analysis of Variance for Res Yield, using Adjusted SS for Tests Source F Umpan IV Umpan Suhu MD F Umpan*IV Umpan F Umpan*Suhu MD IV Umpan*Suhu MD F Umpan*IV Umpan*Suhu MD Error Total

S = 1.12607

DF 2 1 2 2 4 2 4 18 35

R-Sq = 99.43%

Seq SS 3534.34 178.53 261.07 0.08 11.89 6.85 1.61 22.82 4017.21

Adj SS 3534.34 178.53 261.07 0.08 11.89 6.85 1.61 22.82

Adj MS 1767.17 178.53 130.54 0.04 2.97 3.43 0.40 1.27

F 1393.64 140.80 102.94 0.03 2.35 2.70 0.32

P 0.000 0.000 0.000 0.967 0.094 0.094 0.862

R-Sq(adj) = 98.90%

Unusual Observations for Res Yield Obs 7 8

Res Yield 280.600 277.000

Fit 278.800 278.800

SE Fit 0.796 0.796

Residual 1.800 -1.800

St Resid 2.26 R -2.26 R


R denotes an observation with a large standardized residual.

LAMPIRAN – 8B Results for: Worksheet 2 One-way ANOVA: Res Yield_0.6 versus F Umpan_0.6 Source F Umpan_0.6 Error Total S = 2.737

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 1752.48 112.34 1864.83

MS 876.24 7.49

R-Sq = 93.98%

Mean 276.35 288.75 300.52

StDev 2.31 3.35 2.43

F 117.00

P 0.000

R-Sq(adj) = 93.17%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(--*--) (--*--) (--*--) --------+---------+---------+---------+280.0 288.0 296.0 304.0

Pooled StDev = 2.74


F Umpan_0.6 = 5.50 subtracted from: F Umpan_0.6 ----

Lower

Center

Upper

---+---------+---------+---------+--


5.75 6.00 )

9.032 20.799

12.400 24.167

15.768 27.534

(-*--) (--*----+---------+---------+---------+--

----12

0

12

24

F Umpan_0.6 = 5.75 subtracted from: F Umpan_0.6 --6.00

Lower

Center

Upper

---+---------+---------+---------+---

8.399

11.767

15.134

(--*--) ---+---------+---------+---------+---

---12

0

12

24

LAMPIRAN – 8C One-way ANOVA: Res Yield_0.7 versus F Umpan_0.7 Source F Umpan_0.7 Error Total S = 3.577

Level 5.50 5.75 6.00

N 6 6 6

DF 2 15 17

SS 1781.9 191.9 1973.8

MS 891.0 12.8

R-Sq = 90.28%

Mean 280.67 293.28 305.03

StDev 3.01 4.46 3.07

F 69.64

P 0.000

R-Sq(adj) = 88.98%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(---*---) (---*--) (---*---) ---+---------+---------+---------+-----280.0 288.0 296.0 304.0

Pooled StDev = 3.58


F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7 ---5.75 6.00 -)

Lower

Center

Upper

8.210 19.965

12.612 24.367

17.013 28.768

---+---------+---------+---------+-(---*--) (--*----+---------+---------+---------+--

----12

0

12

24

F Umpan_0.7 = 5.75 subtracted from: F Umpan_0.7 --6.00

Lower

Center

Upper

---+---------+---------+---------+---

7.353

11.755

16.157

(---*--) ---+---------+---------+---------+---

---12

0

12

24

LAMPIRAN – 8D Results for: Worksheet 3 One-way ANOVA: Res Yield_5.50 versus IV Umpan_5.50 Source IV Umpan_5.50 Error Total S = 2.683

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 55.90 72.01 127.91

R-Sq = 43.70%

Mean 276.35 280.67

StDev 2.31 3.01

MS 55.90 7.20

F 7.76

P 0.019

R-Sq(adj) = 38.07%

Individual 95% CIs For Mean Based on Pooled StDev ----+---------+---------+---------+----(--------*---------) (---------*--------) ----+---------+---------+---------+----275.0 277.5 280.0 282.5

Pooled StDev = 2.68



All Pairwise Comparisons among Levels of IV Umpan_5.50 Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from: IV Umpan_5.50 ----0.7 ---)

Lower

Center

Upper

--+---------+---------+---------+--

0.865

4.317

7.769

(----------*---------+---------+---------+---------+--

-----3.0

0.0

3.0

6.0

LAMPIRAN – 8E One-way ANOVA: Res Yield_5.75 versus IV Umpan_5.75 Source IV Umpan_5.75 Error Total S = 3.947

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 61.5 155.8 217.3

MS 61.5 15.6

R-Sq = 28.31%

Mean 288.75 293.28

StDev 3.35 4.46

F 3.95

P 0.075

R-Sq(adj) = 21.14%

Individual 95% CIs For Mean Based on Pooled StDev ---------+---------+---------+---------+ (-----------*----------) (-----------*-----------) ---------+---------+---------+---------+ 288.0 291.0 294.0 297.0

Pooled StDev = 3.95




IV Umpan_5.75 = 0.6 subtracted from: IV Umpan_5.75 ----0.7 --)

Lower

Center

Upper

---+---------+---------+---------+-

-0.549

4.528

9.605

(-----------*------------+---------+---------+---------+-

-----4.0

0.0

4.0

8.0

LAMPIRAN – 8F One-way ANOVA: Res Yield_6.00 versus IV Umpan_6.00 Source IV Umpan_6.00 Error Total S = 2.766

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 61.20 76.48 137.68

R-Sq = 44.45%

Mean 300.52 305.03

StDev 2.43 3.07

MS 61.20 7.65

F 8.00

P 0.018

R-Sq(adj) = 38.90%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(---------*---------) (---------*---------) --------+---------+---------+---------+300.0 302.5 305.0 307.5

Pooled StDev = 2.77



IV Umpan_6.00 = 0.6 subtracted from: IV Umpan_6.00 ----0.7 ----)

Lower

Center

Upper

--+---------+---------+---------+--

0.959

4.517

8.074

(-----------*--------+---------+---------+---------+--

-----3.0

0.0

3.0

6.0

LAMPIRAN – 8G Results for: Worksheet 4 One-way ANOVA: Res Yield_218 versus F Umpan_218 Source F Umpan_218 Error Total S = 3.471

Level 5.50 5.75

N 4 4

DF 2 9 11

SS 1183.0 108.4 1291.4

MS 591.5 12.0

R-Sq = 91.60%

Mean 281.40 295.38

StDev 3.44 3.62

F 49.09

P 0.000

R-Sq(adj) = 89.74%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(---*---) (---*---)


6.00

4

305.63

3.35

(---*---) ---+---------+---------+---------+-----300 310 280 290

Pooled StDev = 3.47


F Umpan_218 = 5.50 subtracted from: F Umpan_218 ---5.75 6.00 --)

Lower

Center

Upper

---+---------+---------+---------+--

8.423 18.673

13.975 24.225

19.527 29.777

(----*---) (---*----+---------+---------+---------+--

----12

0

12

24

F Umpan_218 = 5.75 subtracted from: F Umpan_218 --6.00

Lower

Center

Upper

---+---------+---------+---------+---

4.698

10.250

15.802

(----*---) ---+---------+---------+---------+---

---12

0

12

24

LAMPIRAN – 8H One-way ANOVA: Res Yield_220 versus F Umpan_220 Source F Umpan_220 Error Total S = 2.477

Level

N

DF 2 9 11

SS 1237.62 55.20 1292.82

MS 618.81 6.13

R-Sq = 95.73%

Mean

StDev

F 100.89

P 0.000

R-Sq(adj) = 94.78%

Individual 95% CIs For Mean Based on Pooled StDev ------+---------+---------+---------+---


5.50 5.75 6.00

4 4 4

278.13 290.74 303.00

2.78 2.42 2.19

(---*--) (--*---) (---*--) ------+---------+---------+---------+--280.0 288.0 296.0 304.0

Pooled StDev = 2.48


F Umpan_220 = 5.50 subtracted from: F Umpan_220 ---5.75 6.00 *--)

Lower

Center

Upper

8.656 20.913

12.618 24.875

16.579 28.837

----+---------+---------+---------+(---*--) (------+---------+---------+---------+-

----12

0

12

24


Lower

Center

Upper

----+---------+---------+---------+--

8.296

12.257

16.219

(--*---) ----+---------+---------+---------+--

---12

0

12

24

LAMPIRAN – 8I One-way ANOVA: Res Yield_222 versus F Umpan_222 Source F Umpan_222 Error Total

DF 2 9 11

SS 1125.66 46.27 1171.93

MS 562.83 5.14

F 109.47

P 0.000


S = 2.267

Level 5.50 5.75 6.00

N 4 4 4

R-Sq = 96.05%

Mean 276.00 286.93 299.70

StDev 1.83 2.39 2.52

R-Sq(adj) = 95.17%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(--*--) (---*--) (---*--) --------+---------+---------+---------+304.0 280.0 288.0 296.0

Pooled StDev = 2.27


F Umpan_222 = 5.50 subtracted from: F Umpan_222 ---5.75 6.00 -)

Lower

Center

Upper

7.298 20.073

10.925 23.700

14.552 27.327

----+---------+---------+---------+(--*--) (--*----+---------+---------+---------+-

----12

0

12

24


Lower

Center

Upper

----+---------+---------+---------+--

9.148

12.775

16.402

(--*--) ----+---------+---------+---------+--

---12

0

12

24

LAMPIRAN – 8J Results for: Worksheet 5 One-way ANOVA: Res Yield_5.50 versus Suhu MD_5.50


Source Suhu MD_5.50 Error Total S = 2.763

DF 2 9 11

SS 59.20 68.71 127.91

MS 29.60 7.63

R-Sq = 46.28%

F 3.88

P 0.061

R-Sq(adj) = 34.35%

Individual 95% CIs For Mean Based on Pooled StDev Level 218 220 222

N 4 4 4

Mean 281.40 278.13 276.00

StDev 3.44 2.78 1.83

+---------+---------+---------+--------(---------*---------) (---------*----------) (---------*---------) +---------+---------+---------+--------273.0 276.0 279.0 282.0

Pooled StDev = 2.76

Fisher 95% Individual Confidence Intervals All Pairwise Comparisons among Levels of Suhu MD_5.50 Simultaneous confidence level = 88.66%

Suhu MD_5.50 = 218 subtracted from: Suhu MD_5.50 ---220 222

Lower

Center

Upper

+---------+---------+---------+-----

-7.695 -9.820

-3.275 -5.400

1.145 -0.980

(-------*--------) (--------*--------) +---------+---------+---------+-----

----10.0

-5.0

0.0

5.0

Suhu MD_5.50 = 220 subtracted from: Suhu MD_5.50 --222

Lower

Center

Upper

+---------+---------+---------+------

-6.545

-2.125

2.295

(--------*--------) +---------+---------+---------+------

---10.0

-5.0

0.0

5.0

LAMPIRAN – 8K


One-way ANOVA: Res Yield_5.75 versus Suhu MD_5.75 Source Suhu MD_5.75 Error Total S = 2.868

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 143.25 74.03 217.28

MS 71.62 8.23

R-Sq = 65.93%

Mean 295.38 290.74 286.93

StDev 3.62 2.42 2.39

F 8.71

P 0.008

R-Sq(adj) = 58.36%

Individual 95% CIs For Mean Based on Pooled StDev -+---------+---------+---------+-------(-------*--------) (-------*-------) (-------*-------) -+---------+---------+---------+-------284.0 288.0 292.0 296.0

Pooled StDev = 2.87


Suhu MD_5.75 = 218 subtracted from: Suhu MD_5.75 --220 222

Lower

Center

Upper

--+---------+---------+---------+----

-9.220 -13.038

-4.632 -8.450

-0.045 -3.862

(------*-------) (-------*-------) --+---------+---------+---------+----

---12.0

-6.0

0.0

6.0

Suhu MD_5.75 = 220 subtracted from: Suhu MD_5.75 222

Lower

Center

Upper

--+---------+---------+---------+------

-8.405

-3.818

0.770

(-------*------) --+---------+---------+---------+------

-12.0

-6.0

0.0

6.0


LAMPIRAN – 8L One-way ANOVA: Res Yield_6.00 versus Suhu MD_6.00 Source Suhu MD_6.00 Error Total S = 2.732

Level 218 220 222

N 4 4 4

DF 2 9 11

SS 70.52 67.17 137.68

MS 35.26 7.46

R-Sq = 51.22%

Mean 305.63 303.00 299.70

StDev 3.35 2.19 2.52

F 4.72

P 0.040

R-Sq(adj) = 40.37%

Individual 95% CIs For Mean Based on Pooled StDev ---+---------+---------+---------+-----(--------*--------) (--------*--------) (--------*--------) ---+---------+---------+---------+-----297.5 301.0 304.5 308.0

Pooled StDev = 2.73


Suhu MD_6.00 = 218 subtracted from: Suhu MD_6.00 ---220 222

Lower

Center

Upper

-+---------+---------+---------+----

-6.995 -10.295

-2.625 -5.925

1.745 -1.555

(--------*-------) (--------*--------) -+---------+---------+---------+----

----10.0

-5.0

0.0

5.0

Suhu MD_6.00 = 220 subtracted from: Suhu MD_6.00 -222

Lower

Center

Upper

-+---------+---------+---------+------

-7.670

-3.300

1.070

(-------*--------) -+---------+---------+---------+------

--10.0

-5.0

0.0

5.0


LAMPIRAN – 8M Results for: Worksheet 6 One-way ANOVA: Res Yield_0.6 versus Suhu MD_0.6 Source Suhu MD_0.6 Error Total S = 10.87

Level 218 220 222

N 6 6 6

DF 2 15 17

SS 92 1772 1865

MS 46 118

R-Sq = 4.96%

Mean 291.32 288.53 285.77

StDev 10.82 11.39 10.38

F 0.39

P 0.683

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev -----+---------+---------+---------+---(------------*-------------) (------------*-------------) (------------*-------------) -----+---------+---------+---------+---280.0 287.0 294.0 301.0



Suhu MD_0.6 = 218 subtracted from: Suhu MD_0.6 220 222

Lower -16.16 -18.93

Center -2.78 -5.55

Upper 10.59 7.83

---------+---------+---------+---------+ (------------*-------------) (------------*-------------) ---------+---------+---------+---------+ -10 0 10 20


Lower -16.14

Center -2.77

Upper 10.61

---------+---------+---------+---------+ (------------*-------------) ---------+---------+---------+---------+ -10 0 10 20


LAMPIRAN – 8N One-way ANOVA: Res Yield_0.7 versus Suhu MD_0.7 Source Suhu MD_0.7 Error Total S = 10.95

DF 2 15 17

SS 176 1798 1974

MS 88 120

R-Sq = 8.89%

F 0.73

P 0.497

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev Level 218 220 222

N 6 6 6

Mean 296.95 292.71 289.32

StDev 11.05 10.88 10.92

+---------+---------+---------+--------(------------*-------------) (------------*-------------) (------------*-------------) +---------+---------+---------+--------280.0 287.0 294.0 301.0



Suhu MD_0.7 = 218 subtracted from: Suhu MD_0.7 220 222

Lower -17.71 -21.11

Center -4.24 -7.63

Upper 9.24 5.84

-+---------+---------+---------+-------(-------------*------------) (------------*-------------) -+---------+---------+---------+--------20 -10 0 10


Lower -16.87

Center -3.40

Upper 10.08

-+---------+---------+---------+-------(-------------*------------) -+---------+---------+---------+--------20 -10 0 10


LAMPIRAN – 8O Results for: Worksheet 7 One-way ANOVA: Res Yield_218 versus IV Umpan_218 Source IV Umpan_218 Error Total S = 10.94

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 95 1196 1291

MS 95 120

R-Sq = 7.37%

Mean 291.32 296.95

StDev 10.82 11.05

F 0.80

P 0.393

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --------+---------+---------+---------+(-------------*-------------) (-------------*-------------) --------+---------+---------+---------+287.0 294.0 301.0 308.0



IV Umpan_218 = 0.6 subtracted from: IV Umpan_218 --0.7

Lower

Center

Upper

----+---------+---------+---------+--

-8.44

5.63

19.70

(-------------*-------------) ----+---------+---------+---------+--

---10

0

10

20


LAMPIRAN – 8P One-way ANOVA: Res Yield_220 versus IV Umpan_220 Source IV Umpan_220 Error Total S = 11.14

Level 0.6 0.7

N 6 6

DF 1 10 11

SS 52 1240 1293

MS 52 124

R-Sq = 4.05%

Mean 288.53 292.71

StDev 11.39 10.88

F 0.42

P 0.530

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev --+---------+---------+---------+------(-------------*--------------) (-------------*--------------) --+---------+---------+---------+------280.0 287.0 294.0 301.0



IV Umpan_220 = 0.6 subtracted from: IV Umpan_220 ---0.7

Lower

Center

Upper

----+---------+---------+---------+-

-10.15

4.18

18.51

(-------------*--------------) ----+---------+---------+---------+-

----10

0

10

20


LAMPIRAN – 8Q One-way ANOVA: Res Yield_222 versus IV Umpan_222 Source IV Umpan_222 Error Total S = 10.65

DF 1 10 11

SS 38 1134 1172

MS 38 113

R-Sq = 3.23%

F 0.33

P 0.576

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled StDev Level 0.6 0.7

N 6 6

Mean 285.77 289.32

StDev 10.38 10.92

+---------+---------+---------+--------(---------------*---------------) (---------------*---------------) +---------+---------+---------+--------276.0 282.0 288.0 294.0



IV Umpan_222 = 0.6 subtracted from: IV Umpan_222 -+-0.7 ---)

Lower

Center

Upper

-------+---------+---------+--------

-10.15

3.55

17.25

(----------------*--------------------+---------+---------+--------

-+--8.0

0.0

8.0

16.0

————— 12/19/2009 11:02:00 PM ——————————————————


LAMPIRAN -9A

PENGOLAHAN DATA SPC Tabel –L8. Tabel SPC Yield DAS. Pengukuran

Sub

Range

STD BKA

BKB

0.02

90.806

90.781

0.14

90.806

90.781

0.05

0.01

90.806

90.781

0.02

90.836

90.751

0.05

0.04

90.806

90.781

0.02

90.836

90.751

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

0.04

0.05

0.02

90.806

90.781

0.02

90.836

90.751

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

90.794

0.09

0.05

0.05

90.806

90.781

0.02

90.836

90.751

X1

X2

R

R

DEV

Grup

X1

X2

X3

X4

1

90.78

90.77

90.81

90.78

90.785

90.794

0.03

0.05

2

91.00

90.74

90.73

90.72

90.798

90.794

0.28

0.05

3

90.80

90.80

90.78

90.80

90.795

90.794

0.02

4

90.79

90.73

90.83

90.80

90.788

90.794

0.03

5

90.78

90.79

90.80

90.81

90.795

90.794

6

90.77

90.78

90.81

90.80

90.790

90.794

7

90.78

90.80

90.79

90.80

90.793

90.794

8

90.83

90.80

90.77

90.79

90.798

9

90.87

90.78

90.77

90.78

90.800

BKA

BKB

0.02

90.836

90.751

0.02

90.836

90.751

S

10

90.78

90.79

90.78

90.83

90.795

90.794

0.05

0.05

0.02

90.806

90.781

0.02

90.836

90.751

11

90.81

90.79

90.78

90.80

90.795

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

12

90.77

90.80

90.81

90.80

90.795

90.794

0.04

0.05

0.02

90.806

90.781

0.02

90.836

90.751

13

90.80

90.80

90.79

90.80

90.798

90.794

0.01

0.05

0.00

90.806

90.781

0.02

90.836

90.751

14

90.79

90.78

90.79

90.80

90.790

90.794

0.01

0.05

0.01

90.806

90.781

0.02

90.836

90.751

15

90.76

90.80

90.80

90.82

90.795

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

16

90.80

90.81

90.76

90.84

90.803

90.794

0.08

0.05

0.03

90.806

90.781

0.02

90.836

90.751

17

90.81

90.76

90.78

90.80

90.788

90.794

0.05

0.05

0.02

90.806

90.781

0.02

90.836

90.751

18

90.80

90.78

90.79

90.80

90.793

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

19

90.80

90.79

90.78

90.80

90.793

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

20

90.80

90.80

90.80

90.78

90.795

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

21

90.80

90.77

90.78

90.79

90.785

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

22

90.80

90.79

90.77

90.80

90.790

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

23

90.78

90.78

90.81

90.81

90.795

90.794

0.03

0.05

0.02

90.806

90.781

0.02

90.836

90.751


24

90.83

90.79

90.80

90.77

90.798

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

25

90.79

90.79

90.79

90.80

90.793

90.794

0.01

0.05

0.00

90.806

90.781

0.02

90.836

90.751

Untuk X SPC :

Untuk S SPC :

X1= 2269.8 R = 1.15

S = 0.57

X2 = 90.7935 R = 0.05

S = 0.02

n=4

A1 = 1.88

A2 = 0,279

BKA = X2 + A2R = 90.806

BKA = X2 + A1S = 90.836

BKB = X2 – A2R = 90.781

BKA = X2 – A1S = 90.751

LAMPIRAN -9B

PENGOLAHAN DATA SPC Tabel –L9. Data SPC Bilangan Iodium DAS Pengukuran

Sub Grup

X1

X2

X3

Range X4

X1

X2

R

STD R

BKA

BKB

DEV

S

BKA

BKB

1

0.18

0.18

0.17

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

2

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

3

0.18

0.17

0.17

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

4

0.17

0.16

0.18

0.18

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

5

0.18

0.16

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

6

0.18

0.18

0.17

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

7

0.18

0.17

0.18

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

8

0.18

0.17

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

9

0.17

0.17

0.17

0.18

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

10

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

11

0.17

0.18

0.17

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

12

0.18

0.17

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

13

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

14

0.17

0.17

0.18

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

15

0.18

0.18

0.16

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

16

0.18

0.18

0.17

0.16

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

17

0.18

0.17

0.16

0.18

0.173

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

18

0.17

0.18

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

19

0.18

0.18

0.18

0.16

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

20

0.16

0.18

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

21

0.17

0.18

0.18

0.16

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

22

0.18

0.18

0.17

0.18

0.178

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161


23

0.18

0.17

0.18

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

24

0.16

0.18

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

25

0.18

0.16

0.17

0.18

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

Untuk X SPC :

Untuk S SPC :

X1= 4.4

R = 0.3

S = 0.18

X2 = 0.174

R = 0.01

S = 0.01

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 0.178

BKA = X2 + A1S = 0.188

BKB = X2 – A2R = 0.170

BKA = X2 – A1S = 0.161

LAMPIRAN - 9C

PENGOLAHAN DATA SPC Tabel –L10. Data SPC Heat StabilityRed DAS Pengukuran

Sub Grup

X1

Range

X2

X3

X4

X1

X2

R

STD R

BKA

BKB

DEV

S

BKA

BKB

1

0.5

0.5

0.6

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

2

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

3

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

4

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

5

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

6

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

7

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

8

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

9

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

10

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

11

0.5

0.5

0.6

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

12

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

13

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

14

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

15

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

16

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

17

0.5

0.6

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

18

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

19

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

20

0.5

0.6

0.6

0.6

0.575

0.558

0.000

0.096

0.05

0.585

0.531

0.055

0.662

0.454

21

0.6

0.6

0.6

0.5

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454


22

0.6

0.6

0.5

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

23

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

24

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

25

0.6

0.6

0.5

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

Untuk X SPC :

Untuk S SPC :

X1= 14.0

R = 2.4

S = 1.38

X2 = 0.558

R = 0.096

S = 0.06

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 0.585

BKA = X2 + A1S = 0.662

BKB = X2 – A2R = 0.531

BKA = X2 – A1S = 0.454

LAMPIRAN -9D

PENGOLAHAN DATA SPC Tabel –L11. Data SPC Heat Stability Yellow DAS Pengukuran

Sub

Range

STD BKA

BKB

BKA

BKB

0.10

5.47

5.37

0.10

5.47

5.37

0.09

5.585

5.257

0.09

5.585

0.18

0.10

5.47

5.257

5.37

0.09

5.585

0.20

0.18

0.08

5.257

5.47

5.37

0.09

5.585

5.421

0.20

0.18

5.257

0.10

5.47

5.37

0.09

5.585

5.425

5.421

0.20

5.257

0.18

0.10

5.47

5.37

0.09

5.585

5.4

5.400

5.421

5.257

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

5.4

5.4

5.450

5.3

5.4

5.425

5.421

0.10

0.18

0.06

5.47

5.37

0.09

5.585

5.257

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.4

5.4

5.5

5.257

5.450

5.421

0.10

0.18

0.06

5.47

5.37

0.09

5.585

5.257

5.3

5.5

5.5

5.5

5.5

5.4

5.5

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

5.3

5.425

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

13

5.5

5.3

5.257

5.5

5.5

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

14

5.4

5.257

5.4

5.4

5.5

5.425

5.421

0.10

0.18

0.05

5.47

5.37

0.09

5.585

15

5.257

5.5

5.3

5.5

5.4

5.425

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

16

5.5

5.3

5.4

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

17

5.5

5.5

5.3

5.3

5.400

5.421

0.20

0.18

0.12

5.47

5.37

0.09

5.585

5.257

18

5.4

5.4

5.5

5.3

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

19

5.3

5.5

5.4

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

20

5.3

5.4

5.5

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

Grup

X1

X2

R

R

DEV

X1

X2

X3

X4

1

5.3

5.4

5.5

5.5

5.425

5.421

0.20

0.18

2

5.5

5.5

5.4

5.3

5.425

5.421

0.10

0.18

3

5.4

5.5

5.5

5.3

5.425

5.421

0.20

4

5.3

5.4

5.4

5.5

5.400

5.421

5

5.5

5.5

5.3

5.4

5.425

6

5.3

5.4

5.5

5.5

7

5.4

5.3

5.5

8

5.5

5.5

9

5.5

5.5

10

5.5

11 12

S


21

5.3

5.4

5.6

5.4

5.425

5.421

0.20

0.18

0.13

5.47

5.37

0.09

5.585

5.257

22

5.3

5.4

5.5

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

23

5.4

5.4

5.4

5.5

5.425

5.421

0.10

0.18

0.05

5.47

5.37

0.09

5.585

5.257

24

5.5

5.5

5.5

5.3

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

25

5.4

5.5

5.3

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

Untuk X SPC :

Untuk S SPC :

X1= 135.5

R = 4.5

S = 2.18

X2 = 5.421

R = 0.18

S = 0.09

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 5.471

BKA = X2 + A1S = 5.585

BKB = X2 – A2R = 5.371

BKA = X2 – A1S = 5.257

LAMPIRAN -9E

PENGOLAHAN DATA SPC Tabel –L12. Data SPC Bilangan Asam Residue. Pengukuran

Sub Grup 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

X1

X2

X3

24.6 0 24.6 0 24.7 0 24.5 0 24.6 0 24.6 0 24.5 0 24.6 0 24.6 0 24.6 0 24.6 0 24.6 0 24.7 0 24.6 0 24.7 0 24.7 0 24.6 0

24.5 0 24.7 0 24.7 0 24.6 0 24.7 0 24.6 0 24.7 0 24.6 0 24.6 0 24.7 0 24.7 0 24.7 0 24.6 0 24.7 0 24.7 0 24.7 0 24.7 0

24.7 0 24.7 0 24.6 0 24.7 0 24.5 0 24.7 0 24.8 0 24.6 0 24.7 0 24.5 0 24.8 0 24.6 0 24.7 0 24.5 0 24.6 0 24.5 0 24.6 0

X4

X1

X2

Rang e R

STD R

BKA

BKB

DEV

S

BKA

BKB

24.70

24.625

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.50

24.625

24.650

0.30

0.13

0.15

24.687

24.613

0.07

24.785

24.515

24.80

24.650

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.80

24.650

24.650

0.20

0.13

0.13

24.687

24.613

0.07

24.785

24.515

24.60

24.675

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.650

24.650

0.10

0.13

0.06

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.80

24.675

24.650

0.30

0.13

0.13

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515


18 19 20 21 22 23 24 25

24.6 0 24.6 0 24.7 0 24.7 0 24.7 0 24.6 0 24.7 0 24.6 0

24.6 0 24.6 0 24.7 0 24.7 0 24.6 0 24.7 0 24.7 0 24.6 0

24.6 0 24.6 0 24.6 0 24.7 0 24.7 0 24.7 0 24.6 0 24.6 0

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.60

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

Untuk X SPC :

Untuk S SPC :

X1= 616.3

R = 3.3

S = 1.79

X2 = 24.65

R = 0.13

S = 0.07

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 24.687

BKA = X2 + A1S = 24.785

BKB = X2 – A2R = 24.613

BKA = X2 – A1S = 24.515

LAMPIRAN -9F

PENGOLAHAN DATA SPC Tabel –L13. Data SPCYield Residue. Pengukuran

Sub Grup

X1

X2

X3

Range X4

X1

X2

R

STD R

BKA

BKB

DEV

S

BKA

BKB

1

4.96

4.95

4.97

4.97

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

2

4.96

4.97

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

3

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

4

4.95

4.96

4.97

4.97

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

5

4.96

4.97

4.95

4.97

4.963

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

6

4.96

4.96

4.97

4.96

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

7

4.95

4.97

4.98

4.95

4.963

4.965

0.03

0.01

0.02

4.969

4.961

0.01

4.979

4.952

8

4.96

4.96

4.96

4.98

4.965

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

9

4.96

4.96

4.97

4.96

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

10

4.96

4.97

4.95

4.98

4.965

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

11

4.96

4.97

4.98

4.96

4.968

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

12

4.96

4.97

4.96

4.97

4.965

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

13

4.97

4.96

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

14

4.96

4.97

4.95

4.97

4.963

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

15

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952


116

16

4.97

4.97

4.95

4.98

4.968

4.965

0.03

0.01

0.01

4.969

4.961

0.01

4.979

4.952

17

4.96

4.97

4.96

4.96

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

18

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

19

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

20

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952 4.952

21

4.97

4.97

4.97

4.96

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

22

4.97

4.96

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

23

4.96

4.97

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

24

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

25

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

Untuk X SPC :

Untuk S SPC :

X1= 124.1

R = 0.3

S = 0.18

X2 = 4.965

R = 0.01

S = 0.01

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 4.969

BKA = X2 + A1S = 4.979

BKB = X2 – A2R = 4.961

BKA = X2 – A1S = 4.952


LAMPIRAN -1 PROSEDUR ANALISA

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